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@ARTICLE{Patel:618810,
author = {Patel, Jaydeep and Round, Adam and de Wijn, Raphael and
Vakili, Mohammad and Giovanetti, Gabriele and Melo, Diogo
Filipe Monrroy Vilan e and E, Juncheng and Sikorski, Marcin
and Koliyadu, Jayanth and Koua, Faisal H. M. and Sato,
Tokushi and Mancuso, Adrian and Peele, Andrew and Abbey,
Brian},
title = {{R}eal-time analysis of liquid jet sample delivery
stability for an {X}-ray free-electron laser using machine
vision},
journal = {Journal of applied crystallography},
volume = {57},
number = {6},
issn = {1600-5767},
address = {Chester, UK},
publisher = {Wiley-Blackwell},
reportid = {PUBDB-2024-07164},
pages = {1859-1870},
year = {2024},
abstract = {Automated evaluation of optical microscopy images of liquid
jets, commonlyused for sample delivery at X-ray
free-electron lasers (XFELs), enables real-time tracking of
the jet position and liquid jet hit rates, defined here as
theproportion of XFEL pulses intersecting with the liquid
jet. This method utilizesmachine vision for preprocessing,
feature extraction, segmentation and jetdetection as well as
tracking to extract key physical characteristics (such as
thejet angle) from optical microscopy images captured during
experiments. Todetermine the effectiveness of these tools in
monitoring jet stability andenhancing sample delivery
efficiency, we conducted XFEL experiments withvarious sample
compositions (pure water, buffer and buffer with
crystals),nozzle designs and jetting conditions. We
integrated our real-time analysisalgorithm into the Karabo
control system at the European XFEL. The resultsindicate
that the algorithm performs well in monitoring the jet angle
andprovides a quantitative characterization of liquid jet
stability through opticalimage analysis conducted during
experiments},
cin = {$XFEL_E1_SPB/SFX$ / FS-CFEL-1},
ddc = {540},
cid = {$I:(DE-H253)XFEL_E1_SPB_SFX-20210408$ /
I:(DE-H253)FS-CFEL-1-20120731},
pnm = {631 - Matter – Dynamics, Mechanisms and Control
(POF4-631) / 6G13 - Accelerator of European XFEL
(POF4-6G13)},
pid = {G:(DE-HGF)POF4-631 / G:(DE-HGF)POF4-6G13},
experiment = {EXP:(DE-H253)XFEL-Exp-20150101},
typ = {PUB:(DE-HGF)16},
pubmed = {39628876},
UT = {WOS:001387959000015},
doi = {10.1107/S1600576724009853},
url = {https://bib-pubdb1.desy.de/record/618810},
}