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@ARTICLE{Ball:617632,
author = {Ball, O. B. and Husband, R. J. and McHardy, J. D. and
McMahon, M. I. and Strohm, C. and Konôpková, Z. and Appel,
K. and Cerantola, V. and Coleman, A. L. and Cynn, H. and
Dwivedi, A. and Goncharov, A. F. and Graafsma, H. and
Huston, L. Q. and Hwang, H. and Kaa, J. and Kim, J.-Y. and
Koemets, E. and Laurus, T. and Li, X. and Marquardt, H. and
Méndez, A. S. J. and Merkel, S. and Mondal, A. and Morard,
G. and Prakapenka, V. B. and Prescher, C. and Preston, T. R.
and Speziale, S. and Stern, S. and Sturtevant, B. T. and
Sztuk-Dambietz, J. and Velisavljevic, N. and Yoo, C.-S. and
Zastrau, U. and Jenei, Zs. and Liermann, H. P. and
Mcwilliams, Ryan Stewart},
title = {{M}easurement bias in self-heating x-ray free electron
laser experiments from diffraction studies of phase
transformation in titanium},
journal = {Journal of applied physics},
volume = {136},
number = {11},
issn = {0021-8979},
address = {Melville, NY},
publisher = {American Inst. of Physics},
reportid = {PUBDB-2024-06938},
pages = {115902},
year = {2024},
abstract = {X-ray self-heating is a common by-product of X-ray Free
Electron Laser (XFEL) techniques that can affect targets,
optics, and other irradiated materials. Diagnosis of heating
and induced changes in samples may be performed using the
x-ray beam itself as a probe. However, therelationship
between conditions created by and inferred from x-ray
irradiation is unclear and may be highly dependent on the
materialsystem under consideration. Here, we report on a
simple case study of a titanium foil irradiated, heated, and
probed by a MHz XFEL pulsetrain at 18.1 keV delivered by the
European XFEL using measured x-ray diffraction to determine
temperature and finite element analysis tointerpret the
experimental data. We find a complex relationship between
apparent temperatures and sample temperature distributions
thatmust be accounted for to adequately interpret the data,
including beam averaging effects, multivalued temperatures
due to sample phasetransitions, and jumps and gaps in the
observable temperature near phase transformations. The
results have implications for studies employing x-ray
probing of systems with large temperature gradients,
particularly where these gradients are produced by the beam
itself. Finally,this study shows the potential complexity of
studying nonlinear sample behavior, such as phase
transformations, where biasing effects oftemperature
gradients can become paramount, precluding clear observation
of true transformation conditions.},
cin = {XFEL-User / $XFEL_E1_HED$ / FS-HIBEF / FS-DS / FS-PETRA-D},
ddc = {530},
cid = {I:(DE-H253)XFEL-User-20170713 /
$I:(DE-H253)XFEL_E1_HED-20210408$ /
I:(DE-H253)FS-HIBEF-20240110 / I:(DE-H253)FS-DS-20120731 /
I:(DE-H253)FS-PETRA-D-20210408},
pnm = {631 - Matter – Dynamics, Mechanisms and Control
(POF4-631) / DFG project G:(GEPRIS)170172421 - Matter under
extreme conditions as relevant for planetary interior and
dynamo models (170172421)},
pid = {G:(DE-HGF)POF4-631 / G:(GEPRIS)170172421},
experiment = {EXP:(DE-H253)XFEL-SASE2-20150101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:001316241000016},
doi = {10.1063/5.0215908},
url = {https://bib-pubdb1.desy.de/record/617632},
}