Home > Publications database > Resolving Nonequilibrium Shape Variations among Millions of Gold Nanoparticles > print

001     610715
005     20250715170945.0
024 7 _ |a 10.1021/acsnano.4c00378
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024 7 _ |a 1936-0851
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024 7 _ |a arXiv:2401.04896
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088 _ _ |a arXiv:2401.04896
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100 1 _ |a Shen, Zhou
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245 _ _ |a Resolving Nonequilibrium Shape Variations among Millions of Gold Nanoparticles
260 _ _ |a Washington, DC
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520 _ _ |a Nanoparticles, exhibiting functionally relevant structural heterogeneity, are at the forefront of cutting-edge research. Now, high-throughput single-particle imaging (SPI) with X-ray free-electron lasers (XFELs) creates opportunities for recovering the shape distributions of millions of particles that exhibit functionally relevant structural heterogeneity. To realize this potential, three challenges have to be overcome: (1) simultaneous parametrization of structural variability in real and reciprocal spaces; (2) efficiently inferring the latent parameters of each SPI measurement; (3) scaling up comparisons between 10$^5$ structural models and 10$^6$ XFEL-SPI measurements. Here, we describe how we overcame these three challenges to resolve the nonequilibrium shape distributions within millions of gold nanoparticles imaged at the European XFEL. These shape distributions allowed us to quantify the degree of asymmetry in these particles, discover a relatively stable “shape envelope” among nanoparticles, discern finite-size effects related to shape-controlling surfactants, and extrapolate nanoparticles’ shapes to their idealized thermodynamic limit. Ultimately, these demonstrations show that XFEL SPI can help transform nanoparticle shape characterization from anecdotally interesting to statistically meaningful.
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542 _ _ |i 2024-05-29
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773 1 8 |a 10.1021/acsnano.4c00378
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787 0 _ |a Shen, Zhou et.al.
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|t Resolving non-equilibrium shape variations amongst millions of gold nanoparticles
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980 _ _ |a I:(DE-H253)UNI_CUI-20121230
980 _ _ |a I:(DE-H253)UNI_EXP-20120731
980 _ _ |a UNRESTRICTED
980 1 _ |a FullTexts
999 C 5 |a 10.1038/s41570-018-0024-8
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999 C 5 |a 10.1038/s41928-021-00632-7
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999 C 5 |a 10.1021/acs.chemrev.0c00454
|9 -- missing cx lookup --
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999 C 5 |a 10.1021/acs.chemrev.0c00094
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999 C 5 |a 10.1021/nn800264q
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999 C 5 |a 10.1021/ja057254a
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999 C 5 |a 10.1002/adma.201901556
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999 C 5 |a 10.1021/ac0702084
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999 C 5 |a 10.1016/S0032-5910(02)00340-6
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999 C 5 |a 10.1021/cm100458b
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999 C 5 |a 10.1021/nl4043328
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999 C 5 |a 10.1021/cg301445h
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999 C 5 |a 10.1038/nmeth.4347
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999 C 5 |a 10.1146/annurev-biochem-013118-110744
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999 C 5 |a 10.1364/OPTICA.410851
|9 -- missing cx lookup --
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999 C 5 |a 10.1021/acs.jcim.0c00131
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999 C 5 |a 10.1103/PhysRevE.80.026705
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999 C 5 |a 10.1103/PhysRevLett.104.225501
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999 C 5 |a 10.1103/PhysRevLett.114.098102
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999 C 5 |a 10.1107/S1600576716008165
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999 C 5 |a 10.1021/acsnano.0c07961
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999 C 5 |a 10.1364/JOSAA.20.000040
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999 C 5 |2 Crossref
|u Shen, Z. Data Heterogeneity in Single Particle Imaging Experiment with X-ray Free Electron Laser. Ph.D. thesis, National University of Singapore (Singapore), 2021.
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999 C 5 |a 10.1364/OE.21.012385
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999 C 5 |a 10.1038/nphoton.2014.270
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999 C 5 |a 10.1039/C7RA01223C
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999 C 5 |a 10.1021/acs.jpcc.5b07021
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999 C 5 |a 10.1016/S0039-6028(98)00363-X
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999 C 5 |a 10.1007/978-3-642-73902-6
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999 C 5 |a 10.1038/s41598-020-79589-0
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999 C 5 |a 10.1038/nphys3677
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999 C 5 |a 10.1364/OPTICA.416655
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LibraryCollectionCLSMajorCLSMinorLanguageAuthor
Marc 21