Home > Publications database > Effects of Ni doping on structural, magnetic and catalytic properties of copper ferrite > print

001     607712
005     20250723171757.0
024 7 _ |a 10.1016/j.jmmm.2023.171693
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024 7 _ |a 0304-8853
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100 1 _ |a Piskuła, Zbigniew S.
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245 _ _ |a Effects of Ni doping on structural, magnetic and catalytic properties of copper ferrite
260 _ _ |a Amsterdam
|c 2024
|b North-Holland Publ. Co.
336 7 _ |a article
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500 _ _ |a (FP7/2007–2013) under Grant agreement no. 226716.
520 _ _ |a The aim of this work was to obtain information about the influence of small quantities of Ni$^{2+}$ ion on thestructural and magnetic properties of the tetragonally distorted of Cu$_{1-x}$Ni$_x$Fe$_2$O4 series (with x = 0.00, 0.05,0.1, and 0.15 respectively). The tested ferrite system was synthesized by combustion of citrate–nitrate precursors.The synchrotron X-ray diffraction measurements determined the phase transition temperatures (tetragonal →cubic) of all samples. The change of structures under the influence of temperature shows a phase transition in therange of 390 – 400 ◦C for x = 0.00, 330 – 370 ◦C for x = 0.05, 210 – 330 ◦C for x = 0.1 and 140 – 210 ◦C for x= 0.15, respectively. The initial phase transition temperature decreases linearly with the decreasing c/a ratio ofthe crystallographic lattice parameters for the Cu$_{1-x}$Ni$_x$Fe$_2$O$_4$ oxides. Hysteresis measurements were made todetermine the saturation magnetization (M$_S$) and coercive field (μ$_0$H$_c$) of the samples. The values of magneticmoments at room temperature determined from magnetization measurements are very similar to those obtainedfrom theoretical x-ray diffraction calculations. Magnetic moment values per formula unit are estimated to rangefrom 1.16 μB to 1.5 μB. It was found that the catalytic activity of N$_2$O decomposition of samples increases withincreasing nickel content.
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700 1 _ |a Szafran, Maria
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700 1 _ |a Toliński, Tomasz
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