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@ARTICLE{Kilaj:607360,
author = {Kilaj, Ardita and Wang, Jia and Straňák, Patrik and
Schwilk, Max and Rivero, Uxía and Xu, Lei and von
Lilienfeld, O. Anatole and Küpper, Jochen and Willitsch,
Stefan},
title = {{C}onformer-specific polar cycloaddition of
dibromobutadiene with trapped propene ions},
reportid = {PUBDB-2024-01849, arXiv:2107.13858},
year = {2021},
abstract = {Diels-Alder cycloadditions are efficient routes for the
synthesis of cyclic organic compounds. There has been a
long-standing discussion whether these reactions proceed via
stepwise or concerted mechanisms. Here, we adopt a new
experimental approach to explore the mechanistic details of
the model polar cycloaddition of 2,3-dibromo-1,3-butadiene
with propene ions by probing its conformational
specificities in the entrance channel under single-collision
conditions in the gas phase. Combining a conformationally
controlled molecular beam with trapped ions, we find that
both conformers of the diene, gauche and s-trans, are
reactive with capture-limited reaction rates. Aided by
quantum-chemical and quantum-capture calculations, this
finding is rationalised by a simultaneous competition of
concerted and stepwise reaction pathways, revealing an
interesting mechanistic borderline case.},
cin = {FS-CFEL-CMI / UNI/EXP / UNI/CUI},
ddc = {500},
cid = {I:(DE-H253)FS-CFEL-CMI-20220405 /
$I:(DE-H253)UNI_EXP-20120731$ /
$I:(DE-H253)UNI_CUI-20121230$},
pnm = {631 - Matter – Dynamics, Mechanisms and Control
(POF4-631) / DFG project 390715994 - EXC 2056: CUI: Advanced
Imaging of Matter (390715994) / Ex-Net-0002-Phase2-3 -
Advanced Imaging of Matter: Structure, Dynamics and Control
on the Atomic Scale - AIM $(2018_Ex-Net-0002-Phase2-3)$},
pid = {G:(DE-HGF)POF4-631 / G:(GEPRIS)390715994 /
$G:(DE-HGF)2018_Ex-Net-0002-Phase2-3$},
experiment = {EXP:(DE-H253)CFEL-Exp-20150101},
typ = {PUB:(DE-HGF)25},
eprint = {2107.13858},
howpublished = {arXiv:2107.13858},
archivePrefix = {arXiv},
SLACcitation = {$\%\%CITATION$ = $arXiv:2107.13858;\%\%$},
doi = {10.3204/PUBDB-2024-01849},
url = {https://bib-pubdb1.desy.de/record/607360},
}