Home > Publications database > Crystal structures of two new high-pressure oxynitrides with composition SnGe$_4$N$_4$O$_4$, from single-crystal electron diffraction > print

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100 1 _ |a Gollé-Leidreiter, Philipp
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245 _ _ |a Crystal structures of two new high-pressure oxynitrides with composition SnGe$_4$N$_4$O$_4$, from single-crystal electron diffraction
260 _ _ |a Oxford [u.a.]
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520 _ _ |a SnGe$_4$N$_4$O$_4$ was synthesized at high pressure (16 and 20 GPa) and high temperature (1200 and 1500°C) in a large-volume press. Powder X-ray diffraction experiments using synchrotron radiation indicate that the derived samples are mixtures of known and unknown phases. However, the powder X-ray diffraction patterns are not sufficient for structural characterization. Transmission electron microscopy studies reveal crystals of several hundreds of nanometres in size with different chemical composition. Among them, crystals of a previously unknown phase with stoichiometry SnGe$_4$N$_4$O$_4$ were detected and investigated using automated diffraction tomography (ADT), a three-dimensional electron diffraction method. Via ADT, the crystal structure could be determined from single nanocrystals in space group P63mc, exhibiting a nolanite-type structure. This was confirmed by density functional theory calculations and atomic resolution scanning transmission electron microscopy images. In one of the syntheses runs a rhombohedral 6R polytype of SnGe$_4$N$_4$O$_4$ could be found together with the nolanite-type SnGe$_4$N$_4$O$_4$. The structure of this polymorph was solved as well using ADT.
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