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@ARTICLE{Hlderle:601997,
      author       = {Hölderle, Tobias and Monchak, Mykhailo and Baran,
                      Volodymyr and Kriele, Armin and Mühlbauer, Martin J. and
                      Dyadkin, Vadim and Rabenbauer, Alfred and Schökel,
                      Alexander and Ehrenberg, Helmut and Müller-Buschbaum, Peter
                      and Senyshyn, Anatoliy},
      title        = {{T}hermal {S}tructural {B}ehavior of
                      {E}lectrochemically{L}ithiated {G}raphite ({L}i$_x${C}$_6$)
                      {A}nodes in {L}i‐ion {B}atteries},
      journal      = {Batteries $\&$ supercaps},
      volume       = {7},
      number       = {3},
      issn         = {2566-6223},
      address      = {Weinheim},
      publisher    = {Wiley-VCH},
      reportid     = {PUBDB-2024-00457},
      pages        = {e202300499},
      year         = {2024},
      abstract     = {A full series of variously lithiated graphite anodes
                      material Li$_x$C$_6$ (0 < x < 1) corresponding to a
                      different state-of-charge (SOC) between 0 \% and 100 \%
                      was collected from 18650-type cylinder Li-ion batteries, and
                      the thermal structural behavior of these electrodes was
                      mapped using ex situ high-resolution X-ray and neutron
                      diffraction. Their structural behavior was analyzed over a
                      broad temperature range. At high temperatures, a
                      non-reversible decomposition of the lithiated graphite
                      anodes takes place, accompanied by a loss of intercalated
                      lithium ions, forming novel phases such as LiF and Li$_2$O
                      strongly coupled to the degradation of the solid electrolyte
                      interface (SEI). Complementary calorimetric measurements
                      showed the strongly exothermic chemical reactions during the
                      decomposition matching well to the collected diffraction
                      data. Post mortem analysis applying scanning electron
                      microscopy revealed various morphological features
                      supplementing the treatment of battery anodes and
                      highlighted the importance of the SEI layer during the
                      cycling of the cell and its thermal degradation.},
      cin          = {DOOR ; HAS-User / FS-PETRA-D},
      ddc          = {540},
      cid          = {I:(DE-H253)HAS-User-20120731 /
                      I:(DE-H253)FS-PETRA-D-20210408},
      pnm          = {632 - Materials – Quantum, Complex and Functional
                      Materials (POF4-632) / 6G3 - PETRA III (DESY) (POF4-6G3)},
      pid          = {G:(DE-HGF)POF4-632 / G:(DE-HGF)POF4-6G3},
      experiment   = {EXP:(DE-H253)P-P02.1-20150101},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:001158269600001},
      doi          = {10.1002/batt.202300499},
      url          = {https://bib-pubdb1.desy.de/record/601997},
}