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@ARTICLE{Kolmangadi:593057,
author = {Kolmangadi, Mohamed Aejaz and Zhuoqing, Li and Smales, Glen
J. and Pauw, Brian R. and Wuckert, Eugen and Raab, Aileen
and Laschat, Sabine and Huber, Patrick and Schönhals,
Andreas},
title = {{C}onfinement-{S}uppressed {P}hase {T}ransition and
{D}ynamic {S}elf-{A}ssembly of {I}onic {S}uperdiscs in
{O}rdered {N}anochannels: {I}mplications for {N}anoscale
{A}pplications},
journal = {ACS applied nano materials},
volume = {6},
number = {17},
issn = {2574-0970},
address = {Washington, DC},
publisher = {ACS Publications},
reportid = {PUBDB-2023-05260},
pages = {15673 - 15684},
year = {2023},
abstract = {Ionic liquid crystals are ionic liquids that exhibit liquid
crystalline mesomorphism together with ionic conductivity.
As is known, confined liquid crystal mesophases can show
anomalous dynamics and phase behavior. Investigations
considering the factors controlling the macroscopic
properties of ILCs in confinement are rare in the
literature. This study reports the molecular mobility and
the phase transition behavior of a guanidinium-based
columnar ILC confined in the nanopores of self-ordered
anodic aluminum oxide membranes of various pore diameters
(25--180 nm) using broadband dielectric spectroscopy (BDS),
calorimetry, and X-ray scattering. It is aimed at revealing
in which way the pore size as well as the pore surface
wettability (hydrophobic or hydrophilic) alter the molecular
dynamics and phase transition behavior of this system. These
properties are crucial for applications. The DSC
investigations reveal the following: (i) the phase
transition temperature for the transition from the plastic
crystalline to the crystalline-liquid state has nonmonotonic
dependence versus the inverse pore diameter; and (ii) the
transition from the liquid crystalline to the isotropic
phase is suppressed for all nanoconfined samples. This
transition suppressed in the thermal signal was made evident
by BDS and X-ray scattering. It is discussed as a continuous
phase transition taking place in the pores instead of a
discontinuous first-order transition, as observed for the
bulk. BDS investigations show different relaxation processes
for bulk and nanoconfined ILC. The molecular origins of
various relaxation processes are discussed and suggested. It
is further shown that the self-assembly of this ILC is
dynamic in nature, which might apply for other ILCs too. The
obtained results will have implications for nanoscale
applications of ionic liquid crystals.},
cin = {CIMMS},
ddc = {540},
cid = {I:(DE-H253)CIMMS-20211022},
pnm = {632 - Materials – Quantum, Complex and Functional
Materials (POF4-632) / DFG project 430146019 - Ionische
Flüssigkristalle in Nanoporösen Festkörpern:
Selbstorganisation, molekulare Mobilität und
elektro-optische Funktionalitäten (430146019)},
pid = {G:(DE-HGF)POF4-632 / G:(GEPRIS)430146019},
experiment = {EXP:(DE-MLZ)NOSPEC-20140101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:001093805000001},
doi = {10.1021/acsanm.3c02473},
url = {https://bib-pubdb1.desy.de/record/593057},
}