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@ARTICLE{Heck:582119,
author = {Heck, Joshua and Metz, Fabian and Buchenau, Sören and
Teubner, Melissa and Grimm-Lebsanft, Benjamin and Spaniol,
Thomas P. and Hoffmann, Alexander and Rübhausen, Michael A.
and Herres-Pawlis, Sonja},
title = {{M}anipulating electron transfer – the influence of
substituents on novel copper guanidine quinolinyl complexes},
journal = {Chemical science},
volume = {13},
number = {28},
issn = {2041-6520},
address = {Cambridge},
publisher = {RSC},
reportid = {PUBDB-2023-01809},
pages = {8274 - 8288},
year = {2022},
abstract = {Copper guanidine quinolinyl complexes act as good entatic
state models due to their distorted structures leading to a
high similarity between Cu(I) and Cu(II) complexes. For a
better understanding of the entatic state principle
regarding electron transfer a series of guanidine quinolinyl
ligands with different substituents in the 2- and 4-position
were synthesized to examine the influence on the electron
transfer properties of the corresponding copper complexes.
Substituents with different steric or electronic influences
were chosen. The effects on the properties of the copper
complexes were studied applying different experimental and
theoretical methods. The molecular structures of the
bis(chelate) copper complexes were examined in the solid
state by single-crystal X-ray diffraction and in solution by
X-ray absorption spectroscopy and density functional theory
(DFT) calculations revealing a significant impact of the
substituents on the complex structures. For a better insight
natural bond orbital (NBO) calculations of the ligands and
copper complexes were performed. The electron transfer was
analysed by the determination of the electron self-exchange
rates following Marcus theory. The obtained results were
correlated with the results of the structural analysis of
the complexes and of the NBO calculations. Nelsen's
four-point method calculations give a deeper understanding
of the thermodynamic properties of the electron transfer.
These studies reveal a significant impact of the
substituents on the properties of the copper complexes.},
cin = {DOOR ; HAS-User / CFEL-AO},
ddc = {540},
cid = {I:(DE-H253)HAS-User-20120731 / I:(DE-H253)CFEL-AO-20160914},
pnm = {6G3 - PETRA III (DESY) (POF4-6G3)},
pid = {G:(DE-HGF)POF4-6G3},
experiment = {EXP:(DE-H253)P-P64-20150101 / EXP:(DE-H253)P-P65-20150101},
typ = {PUB:(DE-HGF)16},
pubmed = {35919707},
UT = {WOS:000821436200001},
doi = {10.1039/D2SC02910C},
url = {https://bib-pubdb1.desy.de/record/582119},
}