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@ARTICLE{Heinze:491054,
author = {Heinze, Stefan and Krülle, Tim and Ewenz, Lars and Krywka,
Christina and Davydok, Anton and Stark, Andreas and Cremer,
Rainer and Leyens, Christoph},
title = {{I}nfluence of the deposition process and substrate on
microstructure, phase composition, and residual stress state
on as-deposited {C}r-{A}l-{C} coatings},
journal = {Materials and design},
volume = {225},
issn = {0264-1275},
address = {Amsterdam [u.a.]},
publisher = {Elsevier Science},
reportid = {PUBDB-2022-08229},
pages = {111535},
year = {2023},
note = {Preprint is published in Materials $\&$ Design},
abstract = {This paper focuses on the influence of the High Power
Pulsed Magnetron Sputtering (HPPMS) and Direct Current
Magnetron Sputtering (DCMS) coating deposition processes,
the bias voltage, deposition temperature, and substrate on
various properties of the as-deposited state of Cr-Al-C thin
films. Three substrates with different coefficients of
thermal expansion and electrical conductivity were used. To
investigate the microstructure, phase composition, residual
stress state, and mechanical properties, ex-situ and in situ
synchrotron experiments were conducted accompanied by
electron microscopy and nanoindentation. As-deposited
Cr-Al-C coatings consisted of amorphous and crystalline
areas, with the ratio highly dependent on the deposition
process and substrate. The crystalline phase was identified
as metastable (Cr,Al)$_2$C. The highest crystallinity was
determined for DCMS coatings. Increasing temperature and
decreasing bias voltage increased coating crystallinity for
HPPMS coatings. The influence of the deposition process and
bias voltage was highly reduced for the substrate with low
electrical conductivity. In-situ investigations of the
stress state of amorphous areas revealed, that those were
acting as a residual stress buffer. The hardness and
Young’s modulus of the coatings were found to increase
with crystallinity and were slightly increased for
crystalline HPPMS coatings compared to DCMS coatings.},
cin = {DOOR ; HAS-User / UDresden / Hereon},
ddc = {690},
cid = {I:(DE-H253)HAS-User-20120731 / I:(DE-H253)UDresden-20130903
/ I:(DE-H253)Hereon-20210428},
pnm = {6G3 - PETRA III (DESY) (POF4-6G3) / FS-Proposal: I-20170652
(I-20170652) / FS-Proposal: I-20180296 (I-20180296)},
pid = {G:(DE-HGF)POF4-6G3 / G:(DE-H253)I-20170652 /
G:(DE-H253)I-20180296},
experiment = {EXP:(DE-H253)P-P03-20150101 / EXP:(DE-H253)P-P07-20150101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000991089800001},
doi = {10.1016/j.matdes.2022.111535},
url = {https://bib-pubdb1.desy.de/record/491054},
}