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@ARTICLE{Morgenbesser:484450,
author = {Morgenbesser, Maximilian and Viernstein, Alexander and
Schmid, Alexander and Herzig, Christopher and Kubicek,
Markus and Taibl, Stefanie and Bimashofer, Gesara and Stahn,
Jochen and Vaz, Carlos Antonio Fernandes and Döbeli, Max
and Biautti, Federico and de Dios Sirvent, Juan and Liedke,
Maciej Oskar and Butterling, Maik and Kamiński, Michał and
Tolkiehn, Martin and Vonk, Vedran and Stierle, Andreas and
Wagner, Andreas and Tarancon, Albert and Limbeck, Andreas
and Fleig, Jürgen},
title = {{U}nravelling the {O}rigin of {U}ltra‐{L}ow
{C}onductivity in {S}r{T}i{O}$_3$ {T}hin {F}ilms: {S}r
{V}acancies and {T}i on {A}‐{S}ites {C}ause {F}ermi
{L}evel {P}inning},
journal = {Advanced functional materials},
volume = {32},
number = {38},
issn = {1057-9257},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {PUBDB-2022-06265},
pages = {2202226},
year = {2022},
abstract = {Different SrTiO$_3$ thin films are investigated to unravel
the nature of ultra-low conductivities recently found in
SrTiO$_3$ films prepared by pulsed laser deposition.
Impedance spectroscopy reveals electronically
pseudo-intrinsic conductivities for a broad range of
different dopants (Fe, Al, Ni) and partly high dopant
concentrations up to several percent. Using
inductively-coupled plasma optical emission spectroscopy and
reciprocal space mapping, a severe Sr deficiency is found
and positron annihilation lifetime spectroscopy revealed Sr
vacancies as predominant point defects. From
synchrotron-based X-ray standing wave and X-ray absorption
spectroscopy measurements, a change in site occupation is
deduced for Fe-doped SrTiO$_3$ films, accompanied by a
change in the dopant type. Based on these experiments, a
model is deduced, which explains the almost ubiquitous
pseudo-intrinsic conductivity of these films. Sr deficiency
is suggested as key driver by introducing Sr vacancies and
causing site changes (Fe$_{Sr}$ and Ti$_{Sr}$) to
accommodate nonstoichiometry. Sr vacancies act as mid-gap
acceptor states, pinning the Fermi level, provided that
additional donor states (most probably
Ti$_{Sr}^{\bullet\bullet}$) are present. Defect chemical
modeling revealed that such a Fermi level pinning also
causes a self-limitation of the Ti site change and leads to
a very robust pseudo-intrinsic situation, irrespective of
Sr/Ti ratios and doping.},
cin = {DOOR ; HAS-User / FS-PETRA-D / FS-NL},
ddc = {530},
cid = {I:(DE-H253)HAS-User-20120731 /
I:(DE-H253)FS-PETRA-D-20210408 / I:(DE-H253)FS-NL-20120731},
pnm = {632 - Materials – Quantum, Complex and Functional
Materials (POF4-632) / 6G3 - PETRA III (DESY) (POF4-6G3)},
pid = {G:(DE-HGF)POF4-632 / G:(DE-HGF)POF4-6G3},
experiment = {EXP:(DE-H253)P-P24-20150101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000821635900001},
doi = {10.1002/adfm.202202226},
url = {https://bib-pubdb1.desy.de/record/484450},
}