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000476548 245__ $$aBimetallic M$_x$Ru$_{100−x}$ nanoparticles (M = Fe, Co) on supported ionic liquid phases (M$_x$Ru$_{100−x}$@SILP) as hydrogenation catalysts: Influence of M and M:Ru ratio on activity and selectivity
000476548 260__ $$aAmsterdam [u.a.]$$bElsevier$$c2022
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000476548 520__ $$aBimetallic iron-ruthenium and cobalt-ruthenium nanoparticles with systematic variations in the Fe:Ru and Co:Ru ratios are prepared following an organometallic approach and immobilized on an imidazolium-based supported ionic liquid phase (SILP). Resulting MxRu100-x@SILP materials are characterized by electron microscopy, X-ray diffraction and X-ray absorption spectroscopy, confirming the formation of small, well-dispersed and alloyed zero-valent bimetallic nanoparticles. A systematic comparison of the performances of FexRu100−x@SILP and CoxRu100−x@SILP catalysts is made using the hydrogenation of benzilideneacetone as model reaction. The M:Ru ratio is found to have a critical influence on activity and selectivity, with clear synergistic effects arising from the combination of the noble and 3d metals. CoxRu100−x@SILP catalysts are significantly more reactive to reach a given selectivity at a systematically higher content of the 3d metal as compared to the FexRu100−x@SILP catalysts, evidencing a remarkable influence of the nature of the “diluting” 3d metal on the overall performance of the MxRu100−x@SILP catalysts.
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000476548 536__ $$0G:(GEPRIS)390919832$$aDFG project 390919832 - EXC 2186: Das Fuel Science Center – Adaptive Umwandlungssysteme für erneuerbare Energie- und Kohlenstoffquellen (390919832)$$c390919832$$x1
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000476548 7001_ $$0P:(DE-H253)PIP1085616$$aVan Stappen, Casey$$b1
000476548 7001_ $$0P:(DE-H253)PIP1086019$$aRengshausen, Simon$$b2
000476548 7001_ $$0P:(DE-HGF)0$$aHan, Chenhui$$b3
000476548 7001_ $$0P:(DE-H253)PIP1100985$$aSodreau, Alexandre$$b4
000476548 7001_ $$0P:(DE-H253)PIP1023410$$aWeidenthaler, Claudia$$b5
000476548 7001_ $$0P:(DE-HGF)0$$aTricard, Simon$$b6
000476548 7001_ $$0P:(DE-H253)PIP1015325$$aDeBeer, Serena$$b7
000476548 7001_ $$0P:(DE-HGF)0$$aChaudret, Bruno$$b8
000476548 7001_ $$0P:(DE-H253)PIP1086018$$aBordet, Alexis$$b9$$eCorresponding author
000476548 7001_ $$0P:(DE-HGF)0$$aLeitner, Walter$$b10$$eCorresponding author
000476548 773__ $$0PERI:(DE-600)1468993-5$$a10.1016/j.jcat.2022.01.030$$p141 - 148$$tJournal of catalysis$$v407$$x0021-9517$$y2022
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