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@ARTICLE{Chakrabarti:475341,
author = {Chakrabarti, P. and Wildeis, A. and Hartmann, M. and
Brandt, R. and Döhrmann, R. and Fevola, G. and Ossig, C.
and Stuckelberger, M. E. and Garrevoet, J. and Falch, K. V.
and Galbierz, V. and Falkenberg, Gerald and Modregger, P.},
title = {{X}-ray diffraction with micrometer spatial resolution for
highly absorbing samples},
reportid = {PUBDB-2022-01322, arXiv:2201.13264},
year = {2022},
abstract = {X-ray diffraction with high spatial resolution is commonly
used to characterize (poly-)crystalline samples with, for
example, respect to local strain, residual stress, grain
boundaries and texture. However, the investigation of highly
absorbing samples or the simultaneous assessment of high-Z
materials by X-ray fluorescence have been limited due to the
utilisation of low photon energies. Here, we report on a
goniometer-based setup implemented at the P06 beamline of
PETRA III that allows for micrometer spatial resolution with
a photon energy of 35 keV and above. A highly focused beam
was achieved by using compound refractive lenses and high
precision sample manipulation was enabled by a goniometer
that allows for up to 5D scans (3 rotations $\&$ 2
translations). As experimental examples, we demonstrate the
determination of local strain variations in martensitic
steel samples with micrometer spatial resolution as well as
the simultaneous elemental distribution for high-Z materials
in a thin film solar cell. Our proposed approach allows
users from the materials science community to determine
micro-structural properties even in highly absorbing
samples.},
keywords = {Materials Science (cond-mat.mtrl-sci) (Other) / Applied
Physics (physics.app-ph) (Other) / FOS: Physical sciences
(Other)},
cin = {FS-PETRA / FS-PET-S / USiegen},
cid = {I:(DE-H253)FS-PETRA-20140814 / I:(DE-H253)FS-PET-S-20190712
/ I:(DE-H253)USiegen-20120814},
pnm = {632 - Materials – Quantum, Complex and Functional
Materials (POF4-632) / 6G3 - PETRA III (DESY) (POF4-6G3) /
FS-Proposal: I-20200277 (I-20200277)},
pid = {G:(DE-HGF)POF4-632 / G:(DE-HGF)POF4-6G3 /
G:(DE-H253)I-20200277},
experiment = {EXP:(DE-H253)P-P06-20150101},
typ = {PUB:(DE-HGF)25},
eprint = {2201.13264},
howpublished = {arXiv:2201.13264},
archivePrefix = {arXiv},
SLACcitation = {$\%\%CITATION$ = $arXiv:2201.13264;\%\%$},
url = {https://bib-pubdb1.desy.de/record/475341},
}