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@ARTICLE{Brinker:472481,
author = {Brinker, Manuel and Huber, Patrick},
title = {{W}afer-{S}cale {E}lectroactive {N}anoporous {S}ilicon:
{L}arge and {F}ully {R}eversible {E}lectrochemo-{M}echanical
{A}ctuation in {A}queous {E}lectrolytes},
journal = {Advanced materials},
volume = {34},
number = {1},
issn = {0935-9648},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {PUBDB-2021-05034},
pages = {2105923},
year = {2021},
abstract = {Nanoporosity in silicon results in interface-dominated
mechanics, fluidics, and photonics that are often superior
to the ones of the bulk material. However, their active
control, for example, by electronic stimuli, is challenging
due to the absence of intrinsic piezoelectricity in the base
material. Here, for large-scale nanoporous silicon
cantilevers wetted by aqueous electrolytes,
electrosorption-induced mechanical stress generation of up
to 600 kPa that is reversible and adjustable at will by
potential variations of ≈1 V is shown. Laser cantilever
bending experiments in combination with in operando
voltammetry and step coulombmetry allow this large
electro-actuation to be traced to the concerted action of
100 billions of parallel nanopores per square centimeter
cross-section and determination of the capacitive
charge–stress coupling parameter upon ion adsorption and
desorption as well as the intimately related stress
actuation dynamics for perchloric and isotonic saline
solutions. A comparison with planar silicon surfaces reveals
mechanistic insights on the observed electrocapillarity
(Hellmann–Feynman interactions) with respect to the
importance of oxide formation and wall roughness on the
single-nanopore scale. The observation of robust
electrochemo-mechanical actuation in a mainstream
semiconductor with wafer-scale, self-organized nanoporosity
opens up novel opportunities for on-chip integrated stress
generation and actuorics at exceptionally low operation
voltages.},
cin = {TUHH / CIMMS},
ddc = {660},
cid = {I:(DE-H253)TUHH-20210331 / I:(DE-H253)CIMMS-20211022},
pnm = {632 - Materials – Quantum, Complex and Functional
Materials (POF4-632) / EHAWEDRY - Energy harvesting via
wetting/drying cycles with nanoporous electrodes (964524)},
pid = {G:(DE-HGF)POF4-632 / G:(EU-Grant)964524},
experiment = {EXP:(DE-MLZ)NOSPEC-20140101},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:34677879},
UT = {WOS:000709903400001},
doi = {10.1002/adma.202105923},
url = {https://bib-pubdb1.desy.de/record/472481},
}