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@ARTICLE{Weber:460397,
      author       = {Weber, Martin and Balázs, Gábor and Virovets, Alexandr
                      and Peresypkina, Eugenia and Scheer, Manfred},
      title        = {{I}nsertion of {P}hosphenium {I}ons into a
                      {B}icyclo[1.1.0]{T}etraphosphabutane {I}ron {C}omplex},
      journal      = {Molecules},
      volume       = {26},
      number       = {13},
      issn         = {1420-3049},
      address      = {Basel},
      publisher    = {MDPI},
      reportid     = {PUBDB-2021-02915},
      pages        = {3920 (1-13)},
      year         = {2021},
      abstract     = {By reacting [{Cp‴Fe(CO)2}2(µ,η1:1-P4)] (1) with in situ
                      generated phosphenium ions [Ph2P][A] ([A]− = [OTf]− =
                      [O3SCF3]−, [PF6]−), a mixture of two main products of
                      the composition [{Cp‴Fe(CO)2}2(µ,η1:1-P5(C6H5)2)][PF6]
                      (2a and 3a) could be identified by extensive 31P NMR
                      spectroscopic studies at 193 K. Compound 3a was also
                      characterized by X-ray diffraction analysis, showing the
                      rarely observed bicyclo[2.1.0]pentaphosphapentane unit. At
                      room temperature, the novel compound
                      [{Cp‴Fe}(µ,η4:1-P5Ph2){Cp‴(CO)2Fe}][PF6] (4) is formed
                      by decarbonylation. Reacting 1 with in situ generated
                      diphenyl arsenium ions gives short-lived intermediates at
                      193 K which disproportionate at room temperature into
                      tetraphenyldiarsine and
                      [{Cp‴Fe(CO)2}4(µ4,η1:1:1:1-P8)][OTf]2 (5) containing a
                      tetracyclo[3.3.0.02,7.03,6]octaphosphaoctane ligand.},
      cin          = {DOOR ; HAS-User},
      ddc          = {540},
      cid          = {I:(DE-H253)HAS-User-20120731},
      pnm          = {6G3 - PETRA III (DESY) (POF4-6G3) / FS-Proposal: I-20190914
                      (I-20190914)},
      pid          = {G:(DE-HGF)POF4-6G3 / G:(DE-H253)I-20190914},
      experiment   = {EXP:(DE-H253)P-P11-20150101},
      typ          = {PUB:(DE-HGF)16},
      pubmed       = {34206902},
      UT           = {WOS:000670906700001},
      doi          = {10.3390/molecules26133920},
      url          = {https://bib-pubdb1.desy.de/record/460397},
}