% IMPORTANT: The following is UTF-8 encoded.  This means that in the presence
% of non-ASCII characters, it will not work with BibTeX 0.99 or older.
% Instead, you should use an up-to-date BibTeX implementation like “bibtex8” or
% “biber”.

@ARTICLE{Becher:459810,
      author       = {Becher, Johannes and Weber, Sebastian and Ferreira Sanchez,
                      Dario and Doronkin, Dmitry and Garrevoet, Jan and
                      Falkenberg, Gerald and Motta Meira, Debora and Pascarelli,
                      Sakura and Grunwaldt, Jan-Dierk and Sheppard, Thomas L.},
      title        = {{S}ample {E}nvironment for {O}perando {H}ard {X}-ray
                      {T}omography—{A}n {E}nabling {T}echnology for {M}ultimodal
                      {C}haracterization in {H}eterogeneous {C}atalysis},
      journal      = {Catalysts},
      volume       = {11},
      number       = {4},
      issn         = {2073-4344},
      address      = {Basel},
      publisher    = {MDPI},
      reportid     = {PUBDB-2021-02756},
      pages        = {459 (1-18)},
      year         = {2021},
      abstract     = {Structure–activity relations in heterogeneous catalysis
                      can be revealed through in situ and operando measurements of
                      catalysts in their active state. While hard X-ray tomography
                      is an ideal method for non-invasive, multimodal 3D
                      structural characterization on the micron to nm scale,
                      performing tomography under controlled gas and temperature
                      conditions is challenging. Here, we present a flexible
                      sample environment for operando hard X-ray tomography at
                      synchrotron radiation sources. The setup features are
                      discussed, with demonstrations of operando powder X-ray
                      diffraction tomography (XRD-CT) and energy-dispersive
                      tomographic X-ray absorption spectroscopy (ED-XAS-CT).
                      Catalysts for CO$_2$ methanation and partial oxidation of
                      methane are shown as case studies. The setup can be adapted
                      for different hard X-ray microscopy, spectroscopy, or
                      scattering synchrotron radiation beamlines, is compatible
                      with absorption, diffraction, fluorescence, and
                      phase-contrast imaging, and can operate with scanning
                      focused beam or full-field acquisition mode. We present an
                      accessible methodology for operando hard X-ray tomography
                      studies, which offer a unique source of 3D spatially
                      resolved characterization data unavailable to contemporary
                      methods.},
      cin          = {FS-PETRA / FS-PS / KIT / FS-PET-S},
      ddc          = {540},
      cid          = {I:(DE-H253)FS-PETRA-20140814 / I:(DE-H253)FS-PS-20131107 /
                      I:(DE-H253)KIT-20130928 / I:(DE-H253)FS-PET-S-20190712},
      pnm          = {632 - Materials – Quantum, Complex and Functional
                      Materials (POF4-632) / 6G3 - PETRA III (DESY) (POF4-6G3) /
                      FS-Proposal: I-20191105 (I-20191105) / FS-Proposal:
                      I-20190299 (I-20190299)},
      pid          = {G:(DE-HGF)POF4-632 / G:(DE-HGF)POF4-6G3 /
                      G:(DE-H253)I-20191105 / G:(DE-H253)I-20190299},
      experiment   = {EXP:(DE-H253)P-P06-20150101},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000642878200001},
      doi          = {10.3390/catal11040459},
      url          = {https://bib-pubdb1.desy.de/record/459810},
}