guest ::
| Home > Publications database > In situ synchrotron XRD measurements during solidification of a melt in the CaO–SiO$_2$ system using an aerodynamic levitation system > print |
| Home > Publications database > In situ synchrotron XRD measurements during solidification of a melt in the CaO–SiO$_2$ system using an aerodynamic levitation system > print |
| 001 | 459200 | ||
| 005 | 20250716150756.0 | ||
| 024 | 7 | _ | |a 10.1088/1361-648X/abf7e1 |2 doi |
| 024 | 7 | _ | |a 0953-8984 |2 ISSN |
| 024 | 7 | _ | |a 1361-648X |2 ISSN |
| 024 | 7 | _ | |a altmetric:106470630 |2 altmetric |
| 024 | 7 | _ | |a pmid:33853046 |2 pmid |
| 024 | 7 | _ | |a 10.3204/PUBDB-2021-02476 |2 datacite_doi |
| 024 | 7 | _ | |a WOS:000655334500001 |2 WOS |
| 024 | 7 | _ | |2 openalex |a openalex:W3155647922 |
| 037 | _ | _ | |a PUBDB-2021-02476 |
| 041 | _ | _ | |a English |
| 082 | _ | _ | |a 530 |
| 100 | 1 | _ | |a Schraut, Katharina |0 P:(DE-HGF)0 |b 0 |e Corresponding author |
| 245 | _ | _ | |a In situ synchrotron XRD measurements during solidification of a melt in the CaO–SiO$_2$ system using an aerodynamic levitation system |
| 260 | _ | _ | |a Bristol |c 2021 |b IOP Publ. |
| 336 | 7 | _ | |a article |2 DRIVER |
| 336 | 7 | _ | |a Output Types/Journal article |2 DataCite |
| 336 | 7 | _ | |a Journal Article |b journal |m journal |0 PUB:(DE-HGF)16 |s 1622733606_29706 |2 PUB:(DE-HGF) |
| 336 | 7 | _ | |a ARTICLE |2 BibTeX |
| 336 | 7 | _ | |a JOURNAL_ARTICLE |2 ORCID |
| 336 | 7 | _ | |a Journal Article |0 0 |2 EndNote |
| 520 | _ | _ | |a Phase formation and evolution was investigated in the CaO–SiO$_2$ system in the range of 70–80 mol% CaO. The samples were container-less processed in an aerodynamic levitation system and crystallization was followed in situ by synchrotron x-ray diffraction at the beamline P21.1 at the German electron synchrotron (DESY). Modification changes of di- and tricalcium silicate were observed and occurred at lower temperatures than under equilibrium conditions. Despite deep sample undercooling, no metastable phase formation was observed within the measurement timescale of 1 s. For the given cooling rates ranging from 300 K s$^{−1}$ to about 1 K s$^{−1}$, no decomposition of tricalcium silicate was observed. No differences in phase evolution were observed between reducing and oxidizing conditions imposed by the levitation gas (Ar and Ar + O$_2$). We demonstrate that this setup has great potential to followcrystallization in refractory oxide liquids in situ. For sub-second primary phase formation faster detection and for polymorph detection adjustments in resolution have to be implemented. |
| 536 | _ | _ | |a 6G3 - PETRA III (DESY) (POF4-6G3) |0 G:(DE-HGF)POF4-6G3 |c POF4-6G3 |x 0 |f POF IV |
| 536 | _ | _ | |a 632 - Materials – Quantum, Complex and Functional Materials (POF4-632) |0 G:(DE-HGF)POF4-632 |c POF4-632 |x 1 |f POF IV |
| 536 | _ | _ | |a FS-Proposal: I-20191124 (I-20191124) |0 G:(DE-H253)I-20191124 |c I-20191124 |x 2 |
| 588 | _ | _ | |a Dataset connected to CrossRef, Journals: bib-pubdb1.desy.de |
| 693 | _ | _ | |a PETRA III |f PETRA Beamline P21.1 |1 EXP:(DE-H253)PETRAIII-20150101 |0 EXP:(DE-H253)P-P21.1-20150101 |6 EXP:(DE-H253)P-P21.1-20150101 |x 0 |
| 700 | 1 | _ | |a Kargl, Florian |0 P:(DE-HGF)0 |b 1 |
| 700 | 1 | _ | |a Adam, Christian |0 P:(DE-HGF)0 |b 2 |
| 700 | 1 | _ | |a Ivashko, Oleh |0 P:(DE-H253)PIP1025988 |b 3 |u desy |
| 770 | _ | _ | |a Intense Radiation Sources in Condensed Matter and Materials Physics |
| 773 | _ | _ | |a 10.1088/1361-648X/abf7e1 |g Vol. 33, no. 26, p. 264003 - |0 PERI:(DE-600)1472968-4 |n 26 |p 264003 (1-12) |t Journal of physics / Condensed matter |v 33 |y 2021 |x 1361-648X |
| 856 | 4 | _ | |y OpenAccess |u https://bib-pubdb1.desy.de/record/459200/files/Schraut_2021_J._Phys.%20_Condens._Matter_33_264003.pdf |
| 856 | 4 | _ | |y OpenAccess |x pdfa |u https://bib-pubdb1.desy.de/record/459200/files/Schraut_2021_J._Phys.%20_Condens._Matter_33_264003.pdf?subformat=pdfa |
| 909 | C | O | |o oai:bib-pubdb1.desy.de:459200 |p openaire |p open_access |p VDB |p driver |p dnbdelivery |
| 910 | 1 | _ | |a Bundesanstalt für Materialforschung und -prüfung (BAM) |0 I:(DE-HGF)0 |b 0 |6 P:(DE-HGF)0 |
| 910 | 1 | _ | |a Deutsches Zentrum für Luft- und Raumfahrt DLR |0 I:(DE-HGF)0 |b 1 |6 P:(DE-HGF)0 |
| 910 | 1 | _ | |a Bundesanstalt für Materialforschung und -prüfung (BAM) |0 I:(DE-HGF)0 |b 2 |6 P:(DE-HGF)0 |
| 910 | 1 | _ | |a Deutsches Elektronen-Synchrotron |0 I:(DE-588b)2008985-5 |k DESY |b 3 |6 P:(DE-H253)PIP1025988 |
| 913 | 0 | _ | |a DE-HGF |b Forschungsbereich Materie |l Von Materie zu Materialien und Leben |1 G:(DE-HGF)POF3-620 |0 G:(DE-HGF)POF3-621 |3 G:(DE-HGF)POF3 |2 G:(DE-HGF)POF3-600 |4 G:(DE-HGF)POF |v In-house research on the structure, dynamics and function of matter |9 G:(DE-HGF)POF3-6213 |x 0 |
| 913 | 0 | _ | |a DE-HGF |b Forschungsbereich Materie |l Von Materie zu Materialien und Leben |1 G:(DE-HGF)POF3-620 |0 G:(DE-HGF)POF3-622 |3 G:(DE-HGF)POF3 |2 G:(DE-HGF)POF3-600 |4 G:(DE-HGF)POF |v Facility topic: Research on Matter with Brilliant Light Sources |9 G:(DE-HGF)POF3-6G3 |x 1 |
| 913 | 1 | _ | |a DE-HGF |b Forschungsbereich Materie |l Großgeräte: Materie |1 G:(DE-HGF)POF4-6G0 |0 G:(DE-HGF)POF4-6G3 |3 G:(DE-HGF)POF4 |2 G:(DE-HGF)POF4-600 |4 G:(DE-HGF)POF |v PETRA III (DESY) |x 0 |
| 913 | 1 | _ | |a DE-HGF |b Forschungsbereich Materie |l From Matter to Materials and Life |1 G:(DE-HGF)POF4-630 |0 G:(DE-HGF)POF4-632 |3 G:(DE-HGF)POF4 |2 G:(DE-HGF)POF4-600 |4 G:(DE-HGF)POF |v Materials – Quantum, Complex and Functional Materials |x 1 |
| 914 | 1 | _ | |y 2021 |
| 915 | _ | _ | |a DBCoverage |0 StatID:(DE-HGF)0200 |2 StatID |b SCOPUS |d 2021-02-03 |
| 915 | _ | _ | |a DBCoverage |0 StatID:(DE-HGF)0160 |2 StatID |b Essential Science Indicators |d 2021-02-03 |
| 915 | _ | _ | |a DBCoverage |0 StatID:(DE-HGF)1230 |2 StatID |b Current Contents - Electronics and Telecommunications Collection |d 2021-02-03 |
| 915 | _ | _ | |a Creative Commons Attribution CC BY 4.0 |0 LIC:(DE-HGF)CCBY4 |2 HGFVOC |
| 915 | _ | _ | |a JCR |0 StatID:(DE-HGF)0100 |2 StatID |b J PHYS-CONDENS MAT : 2019 |d 2021-02-03 |
| 915 | _ | _ | |a WoS |0 StatID:(DE-HGF)0113 |2 StatID |b Science Citation Index Expanded |d 2021-02-03 |
| 915 | _ | _ | |a DBCoverage |0 StatID:(DE-HGF)0150 |2 StatID |b Web of Science Core Collection |d 2021-02-03 |
| 915 | _ | _ | |a IF < 5 |0 StatID:(DE-HGF)9900 |2 StatID |d 2021-02-03 |
| 915 | _ | _ | |a OpenAccess |0 StatID:(DE-HGF)0510 |2 StatID |
| 915 | _ | _ | |a DBCoverage |0 StatID:(DE-HGF)1150 |2 StatID |b Current Contents - Physical, Chemical and Earth Sciences |d 2021-02-03 |
| 915 | _ | _ | |a National-Konsortium |0 StatID:(DE-HGF)0430 |2 StatID |d 2021-02-03 |w ger |
| 915 | _ | _ | |a DBCoverage |0 StatID:(DE-HGF)0300 |2 StatID |b Medline |d 2021-02-03 |
| 915 | _ | _ | |a Nationallizenz |0 StatID:(DE-HGF)0420 |2 StatID |d 2021-02-03 |w ger |
| 915 | _ | _ | |a DBCoverage |0 StatID:(DE-HGF)0199 |2 StatID |b Clarivate Analytics Master Journal List |d 2021-02-03 |
| 920 | 1 | _ | |0 I:(DE-H253)HAS-User-20120731 |k DOOR ; HAS-User |l DOOR-User |x 0 |
| 920 | 1 | _ | |0 I:(DE-H253)FS-PETRA-D-20210408 |k FS-PETRA-D |l PETRA-D |x 1 |
| 980 | _ | _ | |a journal |
| 980 | _ | _ | |a VDB |
| 980 | _ | _ | |a UNRESTRICTED |
| 980 | _ | _ | |a I:(DE-H253)HAS-User-20120731 |
| 980 | _ | _ | |a I:(DE-H253)FS-PETRA-D-20210408 |
| 980 | 1 | _ | |a FullTexts |
| Library | Collection | CLSMajor | CLSMinor | Language | Author |
|---|