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000459200 1001_ $$0P:(DE-HGF)0$$aSchraut, Katharina$$b0$$eCorresponding author
000459200 245__ $$aIn situ synchrotron XRD measurements during solidification of a melt in the CaO–SiO$_2$ system using an aerodynamic levitation system
000459200 260__ $$aBristol$$bIOP Publ.$$c2021
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000459200 520__ $$aPhase formation and evolution was investigated in the CaO–SiO$_2$ system in the range of 70–80 mol% CaO. The samples were container-less processed in an aerodynamic levitation system and crystallization was followed in situ by synchrotron x-ray diffraction at the beamline P21.1 at the German electron synchrotron (DESY). Modification changes of di- and tricalcium silicate were observed and occurred at lower temperatures than under equilibrium conditions. Despite deep sample undercooling, no metastable phase formation was observed within the measurement timescale of 1 s. For the given cooling rates ranging from 300 K s$^{−1}$ to about 1 K s$^{−1}$, no decomposition of tricalcium silicate was observed. No differences in phase evolution were observed between reducing and oxidizing conditions imposed by the levitation gas (Ar and Ar + O$_2$). We demonstrate that this setup has great potential to followcrystallization in refractory oxide liquids in situ. For sub-second primary phase formation faster detection and for polymorph detection adjustments in resolution have to be implemented.
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000459200 7001_ $$0P:(DE-HGF)0$$aKargl, Florian$$b1
000459200 7001_ $$0P:(DE-HGF)0$$aAdam, Christian$$b2
000459200 7001_ $$0P:(DE-H253)PIP1025988$$aIvashko, Oleh$$b3$$udesy
000459200 770__ $$aIntense Radiation Sources in Condensed Matter and Materials Physics
000459200 773__ $$0PERI:(DE-600)1472968-4$$a10.1088/1361-648X/abf7e1$$gVol. 33, no. 26, p. 264003 -$$n26$$p264003 (1-12)$$tJournal of physics / Condensed matter$$v33$$x1361-648X$$y2021
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