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@ARTICLE{Peresypkina:458619,
author = {Peresypkina, Eugenia and Grill, Kevin and Hiltl, Barbara
and Virovets, Alexandr and Kremer, Werner and Hilgert, Jan
and Tremel, Wolfgang and Scheer, Manfred},
title = {{T}hree‐{C}omponent {S}elf‐{A}ssembly {C}hanges its
{C}ourse: {A} {L}eap from {S}imple {P}olymers to 3{D}
{N}etworks of {S}pherical {H}ost–{G}uest {A}ssemblies},
journal = {Angewandte Chemie / International edition},
volume = {60},
number = {21},
issn = {1521-3773},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {PUBDB-2021-02272},
pages = {12132 - 12142},
year = {2021},
abstract = {One-pot self-assembly reactions of the
polyphosphoruscomplex [Cp*Fe($\eta^5$-P$_5$)] (A), a coinage
metal saltAgSbF$_6$, and flexible aliphatic dinitriles
NC(CH$_2$)$_x$CN (x=1–10) yield 1D, 2D, and 3D
coordination polymers. The sevenmemberedbackbone of the
dinitrile was experimentally foundas the borderline for the
self-assembly system furnishingproducts of different kinds.
At x<7, various rather simplepolymers are exclusively formed
possessing either 0D or 1DAg/A structural motifs connected
by dinitrile spacers, while at x$\geq$+7, the self-assembly
switches to unprecedented extraordinary3D networks of
nano-sized host–guest
assemblies(SbF$_6$)@[(A)$_9$Ag$_{11}$]$^{11+}$ (x=7) or
(A)@[(A)$_{12}$Ag$_{12}$]$^{12+}$ (x=8–10) linked by
dinitriles. The polycationic nodes represent thefirst
superspheres based on A and silver and are host–guestable.
All products are characterized by NMR spectroscopy,mass
spectrometry, and single-crystal X-ray diffraction.
Theassemblies [(A)$_{12}$Ag$_{12}$]$^{12+}$ were visualized
by transmissionelectron microscopy.},
cin = {DOOR ; HAS-User},
ddc = {540},
cid = {I:(DE-H253)HAS-User-20120731},
pnm = {6G3 - PETRA III (DESY) (POF4-6G3) / FS-Proposal: I-20160654
(I-20160654) / FS-Proposal: I-20180967 (I-20180967)},
pid = {G:(DE-HGF)POF4-6G3 / G:(DE-H253)I-20160654 /
G:(DE-H253)I-20180967},
experiment = {EXP:(DE-H253)P-P11-20150101 / EXP:(DE-H253)P-P24-20150101},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:33686782},
UT = {WOS:000646323700001},
doi = {10.1002/anie.202103178},
url = {https://bib-pubdb1.desy.de/record/458619},
}