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@ARTICLE{Bell:456944,
      author       = {Bell, Anthony},
      title        = {{R}ietveld refinement of the low temperature crystal
                      structures of {C}s$_{2}${XS}i$_{5}${O}$_{12}$ ({X}={C}u,
                      {C}d and {Z}n)},
      journal      = {European journal of chemistry},
      volume       = {12},
      number       = {1},
      issn         = {2153-2257},
      address      = {Tucker, Ga.},
      publisher    = {Univ.},
      reportid     = {PUBDB-2021-01769},
      pages        = {60 - 63},
      year         = {2021},
      abstract     = {The synthetic leucite silicate framework mineral analogues
                      Cs$_{2}$XSi$_{5}$O$_{12}$ (X = Cu, Cd, Zn) were prepared by
                      high-temperature solid-state synthesis. The results of
                      Rietveld refinement, using 18 keV synchrotron X-ray powder
                      diffraction data collected at low temperatures (8K X = Cu,
                      Zn; 10K X = Cd) show that the title compounds crystallize in
                      the space group Pbca and are isostructural with the ambient
                      temperature structures of these analogues. The structures
                      consist of tetrahedrally coordinated SiO$_{4}$ and XO$_{4}$
                      sharing corners to form a partially substituted silicate
                      framework. Extraframework Cs cations sit in channels in the
                      framework. All atoms occupy the 8c general position for this
                      space group. In these refined structures, silicon and X
                      atoms are ordered onto separate tetrahedrally coordinated
                      sites (T-sites).},
      cin          = {DOOR ; HAS-User},
      ddc          = {540},
      cid          = {I:(DE-H253)HAS-User-20120731},
      pnm          = {899 - ohne Topic (POF4-899)},
      pid          = {G:(DE-HGF)POF4-899},
      experiment   = {EXP:(DE-H253)D-B2-20150101},
      typ          = {PUB:(DE-HGF)16},
      doi          = {10.5155/eurjchem.12.1.60-63.2089},
      url          = {https://bib-pubdb1.desy.de/record/456944},
}