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000456944 1001_ $$0P:(DE-H253)PIP1011497$$aBell, Anthony$$b0$$eCorresponding author
000456944 245__ $$aRietveld refinement of the low temperature crystal structures of Cs$_{2}$XSi$_{5}$O$_{12}$ (X=Cu, Cd and Zn)
000456944 260__ $$aTucker, Ga.$$bUniv.$$c2021
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000456944 520__ $$aThe synthetic leucite silicate framework mineral analogues Cs$_{2}$XSi$_{5}$O$_{12}$ (X = Cu, Cd, Zn) were prepared by high-temperature solid-state synthesis. The results of Rietveld refinement, using 18 keV synchrotron X-ray powder diffraction data collected at low temperatures (8K X = Cu, Zn; 10K X = Cd) show that the title compounds crystallize in the space group Pbca and are isostructural with the ambient temperature structures of these analogues. The structures consist of tetrahedrally coordinated SiO$_{4}$ and XO$_{4}$ sharing corners to form a partially substituted silicate framework. Extraframework Cs cations sit in channels in the framework. All atoms occupy the 8c general position for this space group. In these refined structures, silicon and X atoms are ordered onto separate tetrahedrally coordinated sites (T-sites).
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