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000454395 1001_ $$0P:(DE-H253)PIP1081881$$aAlbertin, Stefano$$b0$$eCorresponding author
000454395 245__ $$aSurface optical reflectance combined with x-ray techniques during gas-surface interactions
000454395 260__ $$aBristol$$bIOP Publ.$$c2020
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000454395 520__ $$aHigh energy surface x-ray diffraction (HESXRD), x-ray reflectivity (XRR), mass spectrometry (MS) and surface optical reflectance (SOR) have been combined to simultaneously obtain sub-second information on the surface structure and morphology from a Pd(100) model catalyst during in situ oxidation at elevated temperatures and pressures resulting in Pd bulk oxide formation. The results show a strong correlation between the HESXRD and SOR signal intensities during the experiment, enabling phase determination and a time-resolved thickness estimation of the oxide by HESXRD, complemented by XRR measurements. The experiments show a remarkable sensitivity of the SOR to changes in the surface phase and morphology, in particular to the initial stages of oxidation/reduction. The data imply that SOR can detect the formation of an ultrathin PdO surface oxide layer of only 2–3 Å thickness.
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000454395 7001_ $$0P:(DE-H253)PIP1013891$$aGustafson, J.$$b1
000454395 7001_ $$aZhou, J.$$b2
000454395 7001_ $$0P:(DE-H253)PIP1030506$$aPfaff, S.$$b3
000454395 7001_ $$0P:(DE-H253)PIP1017924$$aShipilin, M.$$b4
000454395 7001_ $$0P:(DE-H253)PIP1030501$$aBlomberg, S.$$b5
000454395 7001_ $$0P:(DE-H253)PIP1019770$$aMerte, L. R.$$b6
000454395 7001_ $$0P:(DE-H253)PIP1007064$$aGutowski, Olof$$b7
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000454395 7001_ $$0P:(DE-H253)PIP1030509$$aZetterberg, J.$$b9
000454395 7001_ $$0P:(DE-H253)PIP1013817$$aLundgren, E.$$b10
000454395 7001_ $$0P:(DE-H253)PIP1013630$$aHejral, Uta$$b11$$eCorresponding author
000454395 773__ $$0PERI:(DE-600)1472948-9$$a10.1088/1361-6463/ab77df$$gVol. 53, no. 22, p. 224001 -$$n22$$p224001$$tJournal of physics / D$$v53$$x1361-6463$$y2020
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