Home > Publications database > Synthesis of Na$_{2}$Ti$_{3}$O$_{7}$ nanorods by a V-assisted route and investigation of their battery performance > print

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100 1 _ |a Altin, Serdar
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245 _ _ |a Synthesis of Na$_{2}$Ti$_{3}$O$_{7}$ nanorods by a V-assisted route and investigation of their battery performance
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520 _ _ |a We report the V-assisted synthesis of Na$_2$Ti$_3$O$_7$ nanorods via a conventional solid state reaction technique. Energy dispersive X-ray spectroscopy (EDS) mapping showed that V-ions are not incorporated into the main structure of the nanorods but rather V behaves as a flux agent during the growth of the nanorods. The cyclic voltammetry (CV) analysis of the samples shows changes in the redox peaks as a function of V content. Our detailed ex situ X-ray diffraction (XRD), Raman spectroscopy, scanning electron microscopy (SEM), transmission electron microscopy (TEM) and X-ray absorption spectroscopy (XAS) analyses after 1000 cycles show that the degradation mechanism is the formation of various titanium oxide impurity phases which inhibits the Na-ion diffusion.
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700 1 _ |a Demirel, S.
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700 1 _ |a OZ, E.
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700 1 _ |a Altin, E.
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700 1 _ |a Hetherington, C.
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700 1 _ |a Bayri, A.
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700 1 _ |a Avci, Sevda
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773 _ _ |a 10.1039/C9CE01955C
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