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@ARTICLE{Barranco:454007,
author = {Barranco, Angel and Lopez-Santos, Maria C. and Idigoras,
Jesus and Aparicio, Francisco J. and Obrero-Perez, Jose and
Lopez-Flores, Victor and Contreras-Bernal, Lidia and Rico,
Victor and Ferrer, Javier and Espinos, Juan P. and Borras,
Ana and Anta, Juan A. and Sanchez-Valencia, Juan Ramon},
title = {{E}nhanced {S}tability of {P}erovskite {S}olar {C}ells
{I}ncorporating {D}opant‐{F}ree {C}rystalline
{S}piro‐{OM}e{TAD} {L}ayers by {V}acuum {S}ublimation},
journal = {Advanced energy materials},
volume = {10},
number = {2},
issn = {1614-6840},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {PUBDB-2021-00364},
pages = {1901524},
year = {2020},
abstract = {The main handicap still hindering the eventual exploitation
of organometal halide perovskite‐based solar cells is
their poor stability under prolonged illumination, ambient
conditions, and increased temperatures. This article shows
for the first time the vacuum processing of the most widely
used solid‐state hole conductor (SSHC), i.e., the
Spiro‐OMeTAD [2,2′,7,7′‐tetrakis
(N,N‐di‐p‐methoxyphenyl‐amine)
9,9′‐spirobifluorene], and how its dopant‐free
crystalline formation unprecedently improves perovskite
solar cell (PSC) stability under continuous illumination by
about two orders of magnitude with respect to the
solution‐processed reference and after annealing in air up
to 200 °C. It is demonstrated that the control over the
temperature of the samples during the vacuum deposition
enhances the crystallinity of the SSHC, obtaining a
preferential orientation along the π–π stacking
direction. These results may represent a milestone toward
the full vacuum processing of hybrid organic halide PSCs as
well as light‐emitting diodes, with promising impacts on
the development of durable devices. The microstructure,
purity, and crystallinity of the vacuum sublimated
Spiro‐OMeTAD layers are fully elucidated by applying an
unparalleled set of complementary characterization
techniques, including scanning electron microscopy, X‐ray
diffraction, grazing‐incidence small‐angle X‐ray
scattering and grazing‐incidence wide‐angle X‐ray
scattering, X‐ray photoelectron spectroscopy, and
Rutherford backscattering spectroscopy.},
cin = {DOOR ; HAS-User},
ddc = {050},
cid = {I:(DE-H253)HAS-User-20120731},
pnm = {6G3 - PETRA III (POF3-622) / $NFFA-Europe_supported$ -
Technically supported by Nanoscience Foundries and Fine
Analysis Europe $(2020_Join2-NFFA-Europe_funded)$},
pid = {G:(DE-HGF)POF3-6G3 /
$G:(DE-HGF)2020_Join2-NFFA-Europe_funded$},
experiment = {EXP:(DE-H253)P-P03-20150101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000493839500001},
doi = {10.1002/aenm.201901524},
url = {https://bib-pubdb1.desy.de/record/454007},
}