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@ARTICLE{Joshi:453861,
      author       = {Joshi, Hrishikesh and Ochoa-Hernández, Cristina and
                      Nürenberg, Edward and Kang, Liqun and Wang, Feng Ryan and
                      Weidenthaler, Claudia and Schmidt, Wolfgang and Schüth,
                      Ferdi},
      title        = {{I}nsights into the mechanochemical synthesis of {S}n-β:
                      {S}olid-state metal incorporation in beta zeolite},
      journal      = {Microporous and mesoporous materials},
      volume       = {309},
      issn         = {1387-1811},
      address      = {Amsterdam [u.a.]},
      publisher    = {Elsevier},
      reportid     = {PUBDB-2021-00225},
      pages        = {110566},
      year         = {2020},
      abstract     = {Sn-β zeolite is an active material for the isomerization
                      of glucose to fructose, which is one of the critical
                      reactions for the valorization of biomass. The material is
                      synthesized either by a top-down or bottom-up approach. In
                      this work, we use a top-down approach for the synthesis of
                      Sn-β to incorporate the tin atoms into the *BEA framework.
                      As compared to the literature, we replace the process of
                      manual grinding with the use of ball milling to make the
                      process reproducible, flexible, and scalable. The primary
                      focus of this work is to investigate the processes occurring
                      during the synthesis by a variety of characterization tools.
                      These techniques include thermogravimetric analysis (TGA),
                      X-ray photoelectron spectroscopy (XPS), X-ray absorption
                      spectroscopy (XAS), physisorption, X-ray diffraction (XRD),
                      and chemisorption monitored by Fourier-transform infrared
                      spectroscopy (FTIR). The synthesis is followed by
                      characterizing the material at various stages of synthesis.
                      Finally, the materials are tested for the isomerization of
                      glucose to fructose to assess the chemical nature of Sn-β
                      zeolites. The results of this investigation provide several
                      insights into the mechanochemical process for the
                      incorporation of atoms in a zeolite framework. For instance,
                      the importance of the size of precursors, distribution of Sn
                      atoms during synthesis, and chemical changes occurring
                      during milling are highlighted. These insights could produce
                      a blueprint for the synthesis of a variety of solid
                      catalysts.},
      cin          = {DOOR ; HAS-User},
      ddc          = {530},
      cid          = {I:(DE-H253)HAS-User-20120731},
      pnm          = {6G3 - PETRA III (POF3-622) / FS-Proposal: I-20190358 EC
                      (I-20190358-EC)},
      pid          = {G:(DE-HGF)POF3-6G3 / G:(DE-H253)I-20190358-EC},
      experiment   = {EXP:(DE-H253)P-P64-20150101},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000577314100004},
      doi          = {10.1016/j.micromeso.2020.110566},
      url          = {https://bib-pubdb1.desy.de/record/453861},
}