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@ARTICLE{Chatterjee:453843,
      author       = {Chatterjee, Sayanti and Makai, Szabolcs and Morandi, Bill},
      title        = {{H}ydroxylamine‐{D}erived {R}eagent as a {D}ual {O}xidant
                      and {A}mino {G}roup {D}onor for the {I}ron‐{C}atalyzed
                      {P}reparation of {U}nprotected {S}ulfinamides from {T}hiols},
      journal      = {Angewandte Chemie / International edition},
      volume       = {60},
      number       = {2},
      issn         = {1521-3773},
      address      = {Weinheim},
      publisher    = {Wiley-VCH},
      reportid     = {PUBDB-2021-00207},
      pages        = {758 - 765},
      year         = {2021},
      abstract     = {An iron catalyzed reaction for the selective transformation
                      of thiols (‐SH) to sulfinamides (‐SONH$_2$) by a direct
                      transfer of ‐O and free ‐NH$_2$ groups has been
                      developed. The reaction operates under mild conditions using
                      a bench stable hydroxylamine derived reagent, exhibits broad
                      functional group tolerance, is scalable and proceeds without
                      the use of any precious metal catalyst or additional
                      oxidant. This novel, practical reaction leads to the
                      formation of two distinct new bonds (S=O and S−N) in a
                      single step to chemoselectively form valuable, unprotected
                      sulfinamide products. Preliminary mechanistic studies
                      implicate the role of the alcoholic solvent as an oxygen
                      atom donor.},
      cin          = {DOOR ; HAS-User},
      ddc          = {540},
      cid          = {I:(DE-H253)HAS-User-20120731},
      pnm          = {6G3 - PETRA III (DESY) (POF4-6G3)},
      pid          = {G:(DE-HGF)POF4-6G3},
      experiment   = {EXP:(DE-H253)P-P11-20150101},
      typ          = {PUB:(DE-HGF)16},
      pubmed       = {pmid:32955152},
      UT           = {WOS:000587752700001},
      doi          = {10.1002/anie.202011138},
      url          = {https://bib-pubdb1.desy.de/record/453843},
}