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@MASTERSTHESIS{Striker:449625,
      author       = {Striker, Nele},
      othercontributors = {Gruebel, Gerhard},
      title        = {{D}evelopment of the temperature-controlled sample
                      environment for {D}ouble {P}ulse {P}hoton {C}orrelation
                      {S}pectroscopy},
      school       = {University of Hamburg},
      type         = {Bachelorarbeit},
      reportid     = {PUBDB-2020-03908},
      pages        = {37},
      year         = {2018},
      note         = {Bachelorarbeit, University of Hamburg, 2018},
      abstract     = {A temperature-controlled sample environment was developed
                      and verified for a Double Pulse Photon Correlation
                      Spectroscopy (DPPCS) setup. Various polystyrene and
                      ther-moresponsive Poly(N-Isopropyl Acrylamide) (pNipam)
                      samples were characterized in Dy-namic Light Scattering
                      (DLS) measurements. The thermoresponsive properties of the
                      pNipam sample were investigated in a Small Angle X-Ray
                      Scattering (SAXS) experimentat the beamline P10 of PETRA
                      III. At q≈0.005Å$^{−1}$, an increase in scattered
                      intensitywith increasing temperature was observed,
                      indicating volume (radius) transition of theparticles. To
                      verify the performance of the DPPCS setup in measuring
                      dynamics, thepolystyrene samples were used in Single Pulse
                      Photon Correlation Spectroscopy. Thefastest sample’s
                      radius was determined to R$_h$= 27±3nm, which agrees well
                      with thesize provided by the manufacturer (R= 25±4nm). The
                      pNipam sample was measured attemperatures fromT= 20°C to
                      50°C both with Single and Double Pulse Photon Correla-tion
                      Spectroscopy to verify the performance of the newly
                      developed temperature-control. Both measurements showed the
                      characteristic decrease of the radius at a transition
                      temperature of T≈32°C, demonstrating reliable
                      functionality of the temperature-controlledsample
                      environment},
      cin          = {FS-CXS},
      cid          = {I:(DE-H253)FS-CXS-20130727},
      pnm          = {6212 - Quantum Condensed Matter: Magnetism,
                      Superconductivity (POF3-621)},
      pid          = {G:(DE-HGF)POF3-6212},
      experiment   = {EXP:(DE-MLZ)NOSPEC-20140101},
      typ          = {PUB:(DE-HGF)2},
      doi          = {10.3204/PUBDB-2020-03908},
      url          = {https://bib-pubdb1.desy.de/record/449625},
}