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000439032 1001_ $$0P:(DE-HGF)0$$aArdila-Fierro, Karen J.$$b0
000439032 245__ $$aDirect Visualization of a Mechanochemically Induced Molecular Rearrangement
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000439032 520__ $$aRecent progress in the field of mechanochemistry has expanded the discovery of mechanically induced chemical transformations to several areas of science. However, a general fundamental understanding of how mechanochemical reactions by ball milling occur has remained unreached. For this, we have now implemented in situ monitoring of a mechanochemically induced molecular rearrangement by synchrotron X‐ray powder diffraction, Raman spectroscopy, and real‐time temperature sensing. The results of this study demonstrate that molecular rearrangements can be accomplished in the solid state by ball milling and how in situ monitoring techniques enable the visualization of changes occurring at the exact instant of a molecular migration. The mechanochemical benzil–benzilic acid rearrangement is the focal point of the study. 
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000439032 7001_ $$0P:(DE-H253)PIP1083526$$aLukin, Stipe$$b1
000439032 7001_ $$0P:(DE-H253)PIP1018552$$aEtter, Martin$$b2
000439032 7001_ $$0P:(DE-H253)PIP1026731$$aUžarević, Krunoslav$$b3
000439032 7001_ $$0P:(DE-H253)PIP1085996$$aHalasz, Ivan$$b4
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000439032 7001_ $$0P:(DE-H253)PIP1088073$$aHernandez, Jose$$b6$$eCorresponding author
000439032 773__ $$0PERI:(DE-600)2011836-3$$a10.1002/anie.201914921$$n32$$p13458-13462$$tAngewandte Chemie / International edition International edition$$v59$$x1433-7851$$y2020
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