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@ARTICLE{Kawaguchi:429933,
author = {Kawaguchi, Tomoya and Keller, Thomas F. and Runge, Henning
and Gelisio, Luca and Seitz, Christoph and Kim, Young Yong
and Maxey, Evan R. and Cha, Wonsuk and Ulvestad, Andrew and
Hruszkewycz, Stephan O. and Harder, Ross and Vartanyants,
Ivan A. and Stierle, Andreas and You, Hoydoo},
title = {{G}as-{I}nduced {S}egregation in {P}t-{R}h {A}lloy
{N}anoparticles {O}bserved by {I}n {S}itu {B}ragg
{C}oherent {D}iffraction {I}maging},
journal = {Physical review letters},
volume = {123},
number = {24},
issn = {1079-7114},
address = {College Park, Md.},
publisher = {APS},
reportid = {PUBDB-2019-05420},
pages = {246001},
year = {2019},
note = {© American Physical Society},
abstract = {Bimetallic catalysts can undergo segregation or
redistribution of the metals driven by oxidizing andreducing
environments. Bragg coherent diffraction imaging (BCDI) was
used to relate displacement fieldsto compositional
distributions in crystalline Pt-Rh alloy nanoparticles.
Three-dimensional images ofinternal composition showed that
the radial distribution of compositions reverses partially
between thesurface shell and the core when gas flow changes
between O2 and H2. Our observation suggests that
theelemental segregation of nanoparticle catalysts should be
highly active during heterogeneous catalysis andcan be a
controlling factor in synthesis of electrocatalysts. In
addition, our study exemplifies applications ofBCDI for in
situ 3D imaging of internal equilibrium compositions in
other bimetallic alloy nanoparticles.},
cin = {FS-NL / FS-PS / DOOR ; HAS-User},
ddc = {530},
cid = {I:(DE-H253)FS-NL-20120731 / I:(DE-H253)FS-PS-20131107 /
I:(DE-H253)HAS-User-20120731},
pnm = {6214 - Nanoscience and Materials for Information Technology
(POF3-621) / $NFFA-Europe_supported$ - Technically supported
by Nanoscience Foundries and Fine Analysis Europe
$(2020_Join2-NFFA-Europe_funded)$ / NFFA-Europe -
NANOSCIENCE FOUNDRIES AND FINE ANALYSIS - EUROPE (654360)},
pid = {G:(DE-HGF)POF3-6214 /
$G:(DE-HGF)2020_Join2-NFFA-Europe_funded$ /
G:(EU-Grant)654360},
experiment = {EXP:(DE-H253)Nanolab-04-20150101 /
EXP:(DE-H253)Nanolab-01-20150101},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:31922849},
UT = {WOS:000502798200014},
doi = {10.1103/PhysRevLett.123.246001},
url = {https://bib-pubdb1.desy.de/record/429933},
}