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@ARTICLE{Sarma:426213,
author = {Sarma, Abhisakh and Dippel, Ann-Christin and Gutowski, Olof
and Etter, Martin and Lippmann, Milena and Seeck, Oliver and
Manna, Gouranga and Sanyal, Milan and Keller, Thomas F. and
Kulkarni, Satishkumar and Guha, Puspendu and Satyam,
Parlapali V. and von Zimmermann, Martin},
title = {{E}lectrodeposition of nanowires of a high copper content
thiourea precursor of copper sulfide},
journal = {RSC Advances},
volume = {9},
number = {55},
issn = {2046-2069},
address = {London},
publisher = {RSC Publishing},
reportid = {PUBDB-2019-03632},
pages = {31900 - 31910},
year = {2019},
abstract = {Copper thiourea complexes are an important material class
for application as a precursor of copper sulfidenanocrystals
with potential use in solar cells, optoelectronics,
medicine, etc. They represent a type of singlesource
precursor, comprising both copper and sulfur in one chemical
compound, whose tunablestoichiometry and morphology enable
control of the quality and properties of the synthesized
coppersulfide nanocrystals. Here, we present a template free
electrochemical route to prepare nanowires ofcopper thiourea
(tu) chloride hemihydrate ([Cu(tu)]Cl.1/2H2O) by pulse
deposition. We proposed the modelof the growth of nanowires.
We also demonstrate complete transformation from the
precursor tocopper sulfide nanowire by heating it to 180 C
that involves $20\%$ volume loss due to the decompositionof
organic constituents; the obtained nanowires have around
$38\%$ covellite (CuS) and $62\%$ digenite(Cu1.8S) phases.
Electrochemistry offers the advantage of spatially selected
deposition e.g. in the activeregions of a device.},
cin = {FS-PET-D / FS-NL / DOOR ; HAS-User / FS-TI},
ddc = {540},
cid = {I:(DE-H253)FS-PET-D-20190712 / I:(DE-H253)FS-NL-20120731 /
I:(DE-H253)HAS-User-20120731 / I:(DE-H253)FS-TI-20120731},
pnm = {6G3 - PETRA III (POF3-622) / 6213 - Materials and Processes
for Energy and Transport Technologies (POF3-621) /
INDIA-DESY - INDIA-DESY Collaboration
$(2020_Join2-INDIA-DESY)$},
pid = {G:(DE-HGF)POF3-6G3 / G:(DE-HGF)POF3-6213 /
$G:(DE-HGF)2020_Join2-INDIA-DESY$},
experiment = {EXP:(DE-H253)P-P07-20150101 /
EXP:(DE-H253)Nanolab-04-20150101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000490133300012},
doi = {10.1039/C9RA04293H},
url = {https://bib-pubdb1.desy.de/record/426213},
}