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@ARTICLE{Berlinghof:413959,
author = {Berlinghof, M. and Bär, C. and Haas, D. and Bertram, F.
and Langner, Stefan and Osvet, A. and Chumakov, A. and Will,
J. and Schindler, T. and Zech, T. and Brabec, C. J. and
Unruh, T.},
title = {{F}lexible sample cell for real-time {GISAXS}, {GIWAXS} and
{XRR}: design and construction},
journal = {Journal of synchrotron radiation},
volume = {25},
issn = {1600-5775},
address = {[S.l.]},
publisher = {IUCr},
reportid = {PUBDB-2018-03803},
pages = {1664 - 1672},
year = {2018},
note = {(c) International Union of Crystallography},
abstract = {Since the properties of functional materials are highly
dependent on their specific structure, and since the
structural changes, for example during crystallization,
induced by coating and annealing processes are significant,
the study of structure and its formation is of interest for
fundamental and applied science. However, structure analysis
is often limited to ex situ determination of final states
due to the lack of specialized sample cells that enable
real-time investigations. The lack of such cells is mainly
due to their fairly complex design and geometrical
restrictions defined by the beamline setups. To overcome
this obstacle, an advanced sample cell has been designed and
constructed; it combines automated doctor blading, solvent
vapor annealing and sample hydration with real-time
grazing-incidence wide- and small-angle scattering
(GIWAXS/GISAXS) and X-ray reflectivity (XRR). The sample
cell has limited spatial requirements and is therefore
widely usable at beamlines and laboratory-scale instruments.
The cell is fully automatized and remains portable,
including the necessary electronics. In addition, the cell
can be used by interested scientists in cooperation with the
Institute for Crystallography and Structural Physics and is
expandable with regard to optical secondary probes.
Exemplary research studies are presented, in the form of
coating of P3HT:PC$_{61}$PM thin films, solvent vapor
annealing of DRCN5T:PC$_{71}$BM thin films, and hydration of
supported phospholipid multilayers, to demonstrate the
capabilities of the in situ cell.},
cin = {DOOR ; HAS-User / FS-PE},
ddc = {550},
cid = {I:(DE-H253)HAS-User-20120731 / I:(DE-H253)FS-PE-20120731},
pnm = {6214 - Nanoscience and Materials for Information Technology
(POF3-621) / 6G3 - PETRA III (POF3-622) / DFG project
214951840 - FOR 1878: funCOS - Funktionale molekulare
Strukturen auf komplexen Oxidoberflächen (214951840)},
pid = {G:(DE-HGF)POF3-6214 / G:(DE-HGF)POF3-6G3 /
G:(GEPRIS)214951840},
experiment = {EXP:(DE-H253)P-P08-20150101},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:30407176},
UT = {WOS:000449627100009},
doi = {10.1107/S1600577518013218},
url = {https://bib-pubdb1.desy.de/record/413959},
}