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@ARTICLE{Heymann:408573,
author = {Heymann, Leonard and Schiller, Björn and Noei, Heshmat and
Stierle, Andreas and Klinke, Christian},
title = {{A} {N}ew {S}ynthesis {A}pproach for {C}arbon {N}itrides:
{P}oly(triazine imide) and {I}ts {P}hotocatalytic
{P}roperties},
journal = {ACS omega},
volume = {3},
number = {4},
issn = {2470-1343},
address = {Washington, DC},
publisher = {ACS Publications},
reportid = {PUBDB-2018-02965},
pages = {3892 - 3900},
year = {2018},
abstract = {Poly(triazine imide) (PTI) is a materialbelonging to the
group of carbon nitrides and has shown tohave competitive
properties compared to melon or g-C3N4,especially in
photocatalysis. As most of the carbon nitrides, PTIis
usually synthesized by thermal or hydrothermal approaches.We
present and discuss an alternative synthesis for PTI
whichexhibits a pH-dependent solubility in aqueous
solutions. Thissynthesis is based on the formation of
radicals duringelectrolysis of an aqueous melamine solution,
coupling ofresulting melamine radicals and the final
formation of PTI. Weapplied different characterization
techniques to identify PTI asthe product of this reaction
and report the first liquid stateNMR experiments on a
triazine-based carbon nitride. We showthat PTI has a
relatively high specific surface area and a
pHdependentadsorption of charged molecules. This tunable
adsorption has a significant influence on the photocatalytic
propertiesof PTI, which we investigated in dye degradation
experiments.},
cin = {UNI/PHY / DOOR / FS-NL},
ddc = {540},
cid = {$I:(DE-H253)UNI_PHY-20170505$ /
I:(DE-H253)HAS-User-20120731 / I:(DE-H253)FS-NL-20120731},
pnm = {6213 - Materials and Processes for Energy and Transport
Technologies (POF3-621)},
pid = {G:(DE-HGF)POF3-6213},
experiment = {EXP:(DE-H253)Nanolab-01-20150101 /
EXP:(DE-H253)Nanolab-02-20150101},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:29732448},
UT = {WOS:000430200300030},
doi = {10.1021/acsomega.8b00294},
url = {https://bib-pubdb1.desy.de/record/408573},
}