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@ARTICLE{Paszkowicz:399006,
author = {Paszkowicz, Wojciech and Shekhovtsov, Alexei and Kosmyna,
Miron and Loiko, Pavel and Vilejshikova, Elena and
Minikayev, Roman and Romanowski, Przemysław and
Wierzchowski, Wojciech and Wieteska, Krzysztof and Paulmann,
Carsten and Bryleva, Ekaterina and Belikov, Konstantin and
Fitch, Andrew},
title = {{S}tructure and thermal expansion of
$\mathrm{{C}a_{9}{G}d({VO}_{4})_{7}}$: {A} combined
powder-diffraction and dilatometric study of a
{C}zochralski-grown crystal},
journal = {Nuclear instruments $\&$ methods in physics research / B},
volume = {411},
issn = {0168-583X},
address = {Amsterdam [u.a.]},
publisher = {Elsevier},
reportid = {PUBDB-2018-00323},
pages = {100 - 111},
year = {2017},
note = {(c) Elsevier B.V. ; Post referee fulltext in progress;
Embargo 12 months from publication},
abstract = {Materials of the Ca$_9$RE(VO$_4$)$_7$ (CRVO) formula (RE =
rare earth) and whitlockite-related structures are
considered for applications in optoelectronics, e.g., in
white-light emitting diodes and lasers. In the CRVO
structure, the RE atoms are known to share the site
occupation with Ca atoms at two or three among four Ca
sites, with partial occupancy values depending on the choice
of the RE atom. In this work, the structure and quality of a
Czochralski-grown crystal of this family,
Ca$_9$Gd(VO$_4$)$_7$ (CGVO), are studied using X-ray
diffraction methods. The room-temperature structure is
refined using the powder diffraction data collected at a
high-resolution synchrotron beamline ID22 (ESRF, Grenoble);
for comparison purposes, a laboratory diffraction pattern
was collected and analyzed, as well. The site occupancies
are discussed on the basis of comparison with literature
data of isostructural synthetic crystals of the CRVO series.
The results confirm the previously reported site-occupation
scheme and indicate a tendency of the CGVO compound to adopt
a Gd-deficient composition. Moreover, the thermal expansion
coefficient is determined for CGVO as a function of
temperature in the 302–1023 K range using laboratory
diffraction data. Additionally, for CGVO and six other
single crystals of the same family, thermal expansion is
studied in the 298–473 K range, using the dilatometric
data. The magnitude and anisotropy of thermal expansion,
being of importance for laser applications, are discussed
for these materials.},
cin = {FS-PEX},
ddc = {530},
cid = {I:(DE-H253)FS-PEX-20130206},
pnm = {6213 - Materials and Processes for Energy and Transport
Technologies (POF3-621)},
pid = {G:(DE-HGF)POF3-6213},
experiment = {EXP:(DE-H253)D-F1-20150101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000415772700018},
doi = {10.1016/j.nimb.2017.07.026},
url = {https://bib-pubdb1.desy.de/record/399006},
}