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@ARTICLE{Pospiech:398580,
author = {Pospiech, Doris and Jehnichen, Dieter and Eckstein, Kathrin
and Scheibe, Philipp and Komber, Hartmut and Sahre, Karin
and Janke, Andreas and Reuter, Uta and Häußler, Liane and
Schellkopf, Leonard and Friedel, Peter and Voit, Brigitte},
title = {{S}emifluorinated {PMMA} {B}lock {C}opolymers: {S}ynthesis,
{N}anostructure, and {T}hin {F}ilm {P}roperties},
journal = {Macromolecular chemistry and physics},
volume = {218},
number = {18},
issn = {1022-1352},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {PUBDB-2017-14140},
pages = {1600599 -},
year = {2017},
note = {© WILEY-VCH Verlag GmbH $\&$ Co. KGaA, Weinheim ; Post
referee fulltext in progress; Embargo 12 months from
publication},
abstract = {Diblock copolymers (BCP) with poly(methyl methacrylate) and
poly(1H,1H,2H,2H-perfluorodecyl methacrylate) (PsfMA) blocks
prepared by anionic polymerization in tetrahydrofuran at
−78 °C and atom transfer radical polymerization (ATRP) at
60 °C, respectively, with stepwise varied composition over
a wide range in the phase diagram are compared with respect
to synthesis limits, phase separation behavior in bulk, and
properties of thin films. Both methods yield BCPs with low
dispersity (1.1–1.2) at molar masses below 100 kg
mol$^{−1}$. Higher semifluorinated contents can be
achieved by ATRP in 1,3-bis(trifluoromethyl)benzene which
ensured solubility of PsfMA. BCPs obtained by anionic
polymerization show a more distinct phase separation, that
is, more regular nanostructures. Additionally,
self-organization of the semifluorinated side chains occurs
generating smectic layers which alters in turn the BCP
morphology especially in thin films as compared to
non-semifluorinated BCP. All BCPs show amphiphilic behavior
and form micelles in organic solvents which can be used to
deposit nanoparticles.},
cin = {DOOR},
ddc = {540},
cid = {I:(DE-H253)HAS-User-20120731},
pnm = {899 - ohne Topic (POF3-899)},
pid = {G:(DE-HGF)POF3-899},
experiment = {EXP:(DE-H253)D-A2-20150101 / EXP:(DE-H253)D-BW4-20150101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000410949100009},
doi = {10.1002/macp.201600599},
url = {https://bib-pubdb1.desy.de/record/398580},
}