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@ARTICLE{Terraschke:398019,
      author       = {Terraschke, Huayna and Rothe, Merrit Johanna and
                      Lindenberg, Patric},
      title        = {{I}n situ monitoring metal-ligand exchange processes by
                      optical spectroscopy and {X}-ray diffraction analysis: a
                      review},
      journal      = {Reviews in analytical chemistry},
      volume       = {37},
      number       = {1},
      issn         = {2191-0189},
      address      = {Berlin},
      publisher    = {de Gruyter},
      reportid     = {PUBDB-2017-13636},
      pages        = {20170003},
      year         = {2017},
      abstract     = {Knowledge about the mechanisms involved in the structural
                      development of solid materials at the atomic level is
                      essential for designing rational synthesis protocols for
                      these compounds, which may be used to improve desired
                      technical properties, such as light emission, conductivity,
                      magnetism, porosity or particle size, and may allow the
                      tailored design of solid materials to generate the
                      aforementioned properties. Recent technological advancements
                      have allowed the combination of synchrotron-based in situ
                      X-ray diffraction (XRD) with in situ optical spectroscopy
                      techniques, providing researchers with remarkable
                      opportunities to directly investigate structural changes
                      during synthesis reactions. Among the various available
                      methods to measure optical properties, in situ luminescence,
                      UV/Vis absorption, and light transmission spectroscopies are
                      highlighted here, with in situ luminescence being subdivided
                      into in situ luminescence analysis of coordination sensors
                      (ILACS) and time-resolved laser fluorescence spectroscopy
                      (TRLFS). This article consists of a review of 122 references
                      exploring various aspects of in situ analyses, with
                      particular emphasis on the use of XRD-combined techniques in
                      the study of metal-ligand exchange processes during the
                      formation, phase transitions and decomposition of solid
                      materials, including complexes, coordination polymers,
                      metal-organic frameworks, nanoparticles and polyoxo- or
                      chalcogenide metallates. We will then conclude with an
                      exploration of future trends in this exciting research
                      field.},
      cin          = {DOOR},
      ddc          = {540},
      cid          = {I:(DE-H253)HAS-User-20120731},
      pnm          = {6G3 - PETRA III (POF3-622)},
      pid          = {G:(DE-HGF)POF3-6G3},
      experiment   = {EXP:(DE-H253)P-P09-20150101 / EXP:(DE-H253)P-P07-20150101},
      typ          = {PUB:(DE-HGF)36 / PUB:(DE-HGF)16},
      UT           = {WOS:000427672600001},
      doi          = {10.1515/revac-2017-0003},
      url          = {https://bib-pubdb1.desy.de/record/398019},
}