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@ARTICLE{Eichhorn:331159,
author = {Eichhorn, Klaus D.},
title = {{S}ingle-crystal {X}-ray diffractometry using synchrotron
radiation},
journal = {European journal of mineralogy},
volume = {9},
number = {4},
issn = {0935-1221},
address = {Alexandria, Va.},
publisher = {GeoScienceWorld},
reportid = {PUBDB-2017-07582},
pages = {673 - 692},
year = {1997},
note = {F-Bereich; HASYLAB; no PDF-File},
abstract = {The high brilliance over a wide spectral range up into the
hard X-ray region, the small source size and low divergence,
the polarization properties and the pulsed time structure
are outstanding properties of synchrotron radiation that
extend the range of single-crystal X-ray diffractometry to
experiments which are not feasable with conventional
sources, such as sealed X-ray tube or rotating anode
equipments. There is almost no field of X-ray diffraction
that cannot profit from the use of synchrotron radiation.
Data collection techniques depend on the general goals of a
diffraction experiment, but also on source and beamline
optics, on the sample quality, its absorption and scattering
power, as well as on the instrumental resolution function
and the resulting reflection profile shape. Often, the
sample properties play a crucial role, and not all samples
may be suitable for data collection with synchrotron X-rays.
The high intensity requires detectors with high count-rate
capabilities; area detectors are highly desirable for
high-speed data collection and maximum throughput. The time
dependence of the primary beam intensity and of its
polarization state requires monitoring and normalization to
monitor counts, which complicates data collection and data
reduction due to source of both random and systematic errors
not encountered in conventional X-ray sources. X-ray
diffraction with synchrotron radiation can yield structure
factors of unprecedented quality, provided proper attention
is given to sample properties, data collection strategy and
data evaluation procedures. Synchrotron radiation does not,
however, provide a solution to all problems, in some cases
laboratory X-ray sources may be more appropriate. Given the
limited access to synchrotron radiation facilities, X-ray
diffraction with synchrotron radiation can only supplement,
but not replace conventional X-ray sources and diffraction
techniques.},
cin = {DESY(-2012)},
ddc = {550},
cid = {$I:(DE-H253)DESY_-2012_-20170516$},
pnm = {899 - ohne Topic (POF3-899)},
pid = {G:(DE-HGF)POF3-899},
experiment = {EXP:(DE-MLZ)NOSPEC-20140101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:00},
doi = {10.1127/ejm/9/4/0673},
url = {https://bib-pubdb1.desy.de/record/331159},
}