000292357 001__ 292357 000292357 005__ 20250730113731.0 000292357 0247_ $$2doi$$a10.1016/j.supflu.2015.05.024 000292357 0247_ $$2ISSN$$a0896-8446 000292357 0247_ $$2ISSN$$a1872-8162 000292357 0247_ $$2WOS$$aWOS:000363348500008 000292357 0247_ $$2openalex$$aopenalex:W377059932 000292357 037__ $$aPUBDB-2015-06044 000292357 082__ $$a540 000292357 1001_ $$0P:(DE-HGF)0$$aBehr, Wolfgang$$b0 000292357 245__ $$aSelf diffusion coefficients of organic solvents and their binary mixtures with CO2 in silica alcogels at pressures up to 6MPa derived by NMR pulsed gradient spin echo 000292357 260__ $$aAmsterdam [u.a.]$$bElsevier Science$$c2015 000292357 3367_ $$2DRIVER$$aarticle 000292357 3367_ $$2DataCite$$aOutput Types/Journal article 000292357 3367_ $$0PUB:(DE-HGF)16$$2PUB:(DE-HGF)$$aJournal Article$$bjournal$$mjournal$$s1465401483_12519 000292357 3367_ $$2BibTeX$$aARTICLE 000292357 3367_ $$2ORCID$$aJOURNAL_ARTICLE 000292357 3367_ $$00$$2EndNote$$aJournal Article 000292357 500__ $$a(c) Elsevier B.V. Post referee full text in progress. 000292357 520__ $$aSelf diffusion coefficients were determined using NMR (nuclear magnetic resonance) pulsed gradient spin echo (PGSE) in combination with a special high pressure autoclave. The goal was to determine the self diffusion coefficients for different CO$_{2}$/methanol and CO2/ethanol mixtures within the pore phase of silica alcogels at pressures up to 6 MPa. These values are required as input data for the modeling of process steps preceding the supercritical drying of these gels.The self diffusion coefficients derived with the set-up at 15 °C for unconfined CO$_{2}$/methanol and CO$_{2}$/ethanol mixtures as a function of concentration of the organic solvent as well as of fluid pressure are in line with results from previous publications thus proofing the approach to provide reliable data.Measurements of self diffusion coefficients of methanol at different pressures and methanol/CO$_{2}$ ratios were performed in tetramethoxysilane based silica alcogels with target densities ranging from 80 to 200 kg/m3; the results reveal tortuosities of up to 2.5 depending on the silica fraction in the gel as well as its structure. The experimental self diffusion coefficients are in good agreement with the transport diffusion coefficient determined from time resolved NMR imaging of a fluid exchange within a alcogel of methanol for CO$_{2}$ at 5.8 MPa. 000292357 536__ $$0G:(DE-HGF)POF3-899$$a899 - ohne Topic (POF3-899)$$cPOF3-899$$fPOF III$$x0 000292357 588__ $$aDataset connected to CrossRef 000292357 693__ $$0EXP:(DE-H253)D-B1-20150101$$1EXP:(DE-H253)DORISIII-20150101$$6EXP:(DE-H253)D-B1-20150101$$aDORIS III$$fDORIS Beamline B1$$x0 000292357 7001_ $$0P:(DE-HGF)0$$aBehr, Volker C.$$b1 000292357 7001_ $$0P:(DE-H253)PIP1010896$$aReichenauer, G.$$b2$$eCorresponding author 000292357 773__ $$0PERI:(DE-600)2021726-2$$a10.1016/j.supflu.2015.05.024$$gVol. 106, p. 50 - 56$$p50 - 56$$tThe journal of supercritical fluids$$v106$$x0896-8446$$y2015 000292357 8564_ $$uhttps://bib-pubdb1.desy.de/record/292357/files/10.1016_j.supflu.2015.05.024.pdf$$yRestricted 000292357 8564_ $$uhttps://bib-pubdb1.desy.de/record/292357/files/10.1016_j.supflu.2015.05.024.gif?subformat=icon$$xicon$$yRestricted 000292357 8564_ $$uhttps://bib-pubdb1.desy.de/record/292357/files/10.1016_j.supflu.2015.05.024.jpg?subformat=icon-1440$$xicon-1440$$yRestricted 000292357 8564_ $$uhttps://bib-pubdb1.desy.de/record/292357/files/10.1016_j.supflu.2015.05.024.jpg?subformat=icon-180$$xicon-180$$yRestricted 000292357 8564_ $$uhttps://bib-pubdb1.desy.de/record/292357/files/10.1016_j.supflu.2015.05.024.jpg?subformat=icon-640$$xicon-640$$yRestricted 000292357 8564_ $$uhttps://bib-pubdb1.desy.de/record/292357/files/10.1016_j.supflu.2015.05.024.pdf?subformat=pdfa$$xpdfa$$yRestricted 000292357 909CO $$ooai:bib-pubdb1.desy.de:292357$$pVDB 000292357 9101_ $$0I:(DE-HGF)0$$6P:(DE-H253)PIP1010896$$aExternes Institut$$b2$$k>Extern 000292357 9131_ $$0G:(DE-HGF)POF3-899$$1G:(DE-HGF)POF3-890$$2G:(DE-HGF)POF3-800$$3G:(DE-HGF)POF3$$4G:(DE-HGF)POF$$aDE-HGF$$bProgrammungebundene Forschung$$lohne Programm$$vohne Topic$$x0 000292357 9141_ $$y2015 000292357 915__ $$0StatID:(DE-HGF)0420$$2StatID$$aNationallizenz 000292357 915__ $$0StatID:(DE-HGF)0300$$2StatID$$aDBCoverage$$bMedline 000292357 915__ $$0StatID:(DE-HGF)0100$$2StatID$$aJCR$$bJ SUPERCRIT FLUID : 2014 000292357 915__ $$0StatID:(DE-HGF)0200$$2StatID$$aDBCoverage$$bSCOPUS 000292357 915__ $$0StatID:(DE-HGF)0199$$2StatID$$aDBCoverage$$bThomson Reuters Master Journal List 000292357 915__ $$0StatID:(DE-HGF)0110$$2StatID$$aWoS$$bScience Citation Index 000292357 915__ $$0StatID:(DE-HGF)0150$$2StatID$$aDBCoverage$$bWeb of Science Core Collection 000292357 915__ $$0StatID:(DE-HGF)0111$$2StatID$$aWoS$$bScience Citation Index Expanded 000292357 915__ $$0StatID:(DE-HGF)1150$$2StatID$$aDBCoverage$$bCurrent Contents - Physical, Chemical and Earth Sciences 000292357 915__ $$0StatID:(DE-HGF)1160$$2StatID$$aDBCoverage$$bCurrent Contents - Engineering, Computing and Technology 000292357 915__ $$0StatID:(DE-HGF)9900$$2StatID$$aIF < 5 000292357 9201_ $$0I:(DE-H253)HAS-User-20120731$$kDOOR$$lDOOR-User$$x0 000292357 980__ $$ajournal 000292357 980__ $$aVDB 000292357 980__ $$aI:(DE-H253)HAS-User-20120731 000292357 980__ $$aUNRESTRICTED