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@ARTICLE{Legrand:207294,
author = {Legrand, Stijn and Alfeld, Matthias and Vanmeert, Frederik
and De Nolf, Wout and Janssens, Koen},
title = {{M}acroscopic {F}ourier {T}ransform {I}nfrared {S}canning
in {R}eflection {M}ode ({MA}-r{FTIR}), a new {T}ool for
{C}hemical {I}maging of {C}ultural {H}eritage {A}rtefacts in
the {M}id-{I}nfrared {R}ange},
journal = {The analyst},
volume = {139},
number = {10},
issn = {1364-5528},
address = {Cambridge},
publisher = {Soc.},
reportid = {PUBDB-2015-01277},
pages = {2489},
year = {2014},
note = {(c) Royal Society of Chemistry. Post referee full text in
progress.},
abstract = {In this paper we demonstrate that by means of scanning
reflection FTIR spectroscopy, it is possible to record
highly specific distribution maps of organic and inorganic
compounds from flat, macroscopic objects with cultural
heritage value in a non-invasive manner. Our previous work
involved the recording of macroscopic distributions of
chemical elements or crystal phases from painted works of
art based on respectively macroscopic X-ray fluorescence or
X-ray powder diffraction analysis. The use of infrared
radiation instead of X-rays has the advantage that more
specific information about the nature and distribution of
the chemical compounds present can be gathered. This higher
imaging specificity represents a clear advantage for the
characterization of painting and artist materials. It allows
the distribution of metallo-organic compounds to be
visualized and permits distinguishing between pigmented
materials containing the same key metal. The prototype
instrument allows the recording of hyperspectral datacubes
by scanning the surface of the artefact in a contactless and
sequential single-point measuring mode, while recording the
spectrum of reflected infrared radiation. After the
acquisition, spectral line intensities of individual bands
and chemical distribution maps can be extracted from the
datacube to identify the compounds present and/or to
highlight their spatial distribution. Not only is
information gained on the surface of the investigated
artefacts, but also images of overpainted paint layers and,
if present, the underdrawing may be revealed in this manner.
A current major limitation is the long scanning times
required to record these maps.},
cin = {DOOR / FS-PE},
ddc = {540},
cid = {I:(DE-H253)HAS-User-20120731 / I:(DE-H253)FS-PE-20120731},
pnm = {FS In-house research / external facilities (POF2-544)},
pid = {G:(DE-H253)POF2-Other-Beam-20130405},
experiment = {EXP:(DE-MLZ)External-20140101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000334734200028},
pubmed = {pmid:24665463},
doi = {10.1039/c3an02094k},
url = {https://bib-pubdb1.desy.de/record/207294},
}