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@ARTICLE{Hunter:207279,
author = {Hunter, Mark S. and Segelke, Brent and Messerschmidt, Marc
and Williams, Garth J. and Zatsepin, Nadia A. and Barty,
Anton and Benner, W. Henry and Carlson, David B. and
Coleman, Matthew and Graf, Alexander and Hau-Riege, Stefan
P. and Pardini, Tommaso and Seibert, M. Marvin and Evans,
James and Boutet, Sébastien and Frank, Matthias},
title = {{F}ixed-{T}arget {P}rotein {S}erial {M}icrocrystallography
with an {X}-ray {F}ree {E}lectron {L}aser},
journal = {Scientific reports},
volume = {4},
number = {6026},
issn = {2045-2322},
address = {London},
publisher = {Nature Publishing Group},
reportid = {PUBDB-2015-01262},
pages = {1},
year = {2014},
note = {OA},
abstract = {We present results from experiments at the Linac Coherent
Light Source (LCLS) demonstrating that serial femtosecond
crystallography (SFX) can be performed to high resolution
(~2.5 Å) using protein microcrystals deposited on an
ultra-thin silicon nitride membrane and embedded in a
preservation medium at room temperature. Data can be
acquired at a high acquisition rate using x-ray free
electron laser sources to overcome radiation damage, while
sample consumption is dramatically reduced compared to
flowing jet methods. We achieved a peak data acquisition
rate of 10 Hz with a hit rate of $~38\%,$ indicating that
a complete data set could be acquired in about one 12-hour
LCLS shift using the setup described here, or in even less
time using hardware optimized for fixed target SFX. This
demonstration opens the door to ultra low sample consumption
SFX using the technique of diffraction-before-destruction on
proteins that exist in only small quantities and/or do not
produce the copious quantities of microcrystals required for
flowing jet methods.},
cin = {FS-CFEL-1},
ddc = {000},
cid = {I:(DE-H253)FS-CFEL-1-20120731},
pnm = {Experiments at CFEL (POF2-544)},
pid = {G:(DE-H253)POF2-CFEL-Exp.-20130405},
experiment = {EXP:(DE-H253)CFEL-Exp-20150101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000340674000004},
pubmed = {pmid:25113598},
doi = {10.1038/srep06026},
url = {https://bib-pubdb1.desy.de/record/207279},
}