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@ARTICLE{Uchida:206066,
author = {Uchida, H. T. and Wagner, S. and Hamm, M. and Kürschner,
J. and Kirchheim, R. and Hjörvarsson, B. and Pundt, A.},
title = {{A}bsorption kinetics and hydride formation in magnesium
films: {E}ffect of driving force revisited},
journal = {Acta materialia},
volume = {85},
issn = {1359-6454},
address = {Amsterdam [u.a.]},
publisher = {Elsevier Science},
reportid = {PUBDB-2015-00599},
pages = {279 - 289},
year = {2015},
abstract = {Electrochemical hydrogen permeation measurements and in
situ gas-loading X-ray diffraction measurements were
performed on polycrystalline Mg films. Hydrogen diffusion
constants, the hydride volume content and the in-plane
stress were determined for different values of driving
forces at 300 K. For α-Mg–H, a hydrogen diffusion
constant of View the MathML sourceDHMg=7(±2)·10-11 m2
s−1 was determined. For higher concentrations, different
kinetic regimes with reduced apparent diffusion constants
View the MathML sourceDHtot were found, depending on the
driving force, decreasing to about View the MathML
sourceDHtot = 10−18 m2 s−1. This lowest measured
diffusion constant is two orders of magnitude larger than
that of bulk β-MgH2, and the difference is ascribed to a
contribution from a fast diffusion along grain boundaries.
The different kinetics regimes are attributed to the spatial
distribution of hydrides. A heterogeneous hydride nucleation
and growth model is suggested that is based on hemispherical
hydrides spatially distributed according to the nuclei
densities expressed as a function of the driving force. The
model allows us to qualitatively explain the complex stress
development, the different diffusion regimes and the
blocking-layer thickness. As the blocking-layer thickness
inversely scales with the driving force, small driving
forces allow the hydriding of large film volume fractions.
Maximum stress situations occur for hydride distances
reaching four times the hydride radius and for hydride
distances equaling the film thickness.},
cin = {DOOR},
ddc = {670},
cid = {I:(DE-H253)HAS-User-20120731},
pnm = {6G3 - PETRA III (POF3-622) / FS-Proposal: II-20100323 EC
(II-20100323-EC) / FS-Proposal: I-20120283 (I-20120283)},
pid = {G:(DE-HGF)POF3-6G3 / G:(DE-H253)II-20100323-EC /
G:(DE-H253)I-20120283},
experiment = {EXP:(DE-H253)D-B2-20150101 / EXP:(DE-H253)P-P08-20150101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000348956800028},
doi = {10.1016/j.actamat.2014.11.031},
url = {https://bib-pubdb1.desy.de/record/206066},
}