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000171851 1001_ $$0P:(DE-H253)PIP1013348$$aMichels, Rolf$$b0
000171851 245__ $$aCoaggregation of Two Anionic Azo Dyestuffs: A Combined Static Light Scattering and Small-Angle X-ray Scattering Study
000171851 260__ $$aWashington, DC$$bSoc.$$c2014
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000171851 520__ $$aThe formation of azo dyestuff aggregates in dilute aqueous solution induced by the addition of Mg2+, Ca2+, Sr2+, or Ba2+ ions is followed by time-resolved static light scattering (SLS) and time-resolved small-angle X-ray scattering (SAXS). Time-dependent molar mass data of the growing aggregates is interpreted by means of a kinetic model introduced by Lomakin et al. ( Proc. Natl. Acad. Sci. U.S.A. 1996, 93, 1125) for the description of β-amyloid aggregation. This interpretation reveals significant trends within the homologous series of alkaline earth cations. The trends refer to the nucleation and the growth rate of the dyestuff fibers. Time-resolved SAXS experiments indicate that these first two stages are followed by a third one during which a network forms by partial lateral alignment of fibers. At high enough dyestuff concentrations, this network formation even leads to a gel-like phase. Anomalous SAXS (ASAXS) on such a gel phase formed upon the addition of Sr2+ revealed the extent of neutralization of the dyestuff molecules within the gel by the specifically interacting alkaline earth cations.
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000171851 7001_ $$0P:(DE-HGF)0$$aGoerigk, Günter$$b1
000171851 7001_ $$0P:(DE-H253)PIP1005990$$aVainio, Ulla$$b2
000171851 7001_ $$0P:(DE-HGF)0$$aGummel, Jérémie$$b3
000171851 7001_ $$0P:(DE-H253)PIP1008904$$aHuber, Klaus$$b4$$eCorresponding Author
000171851 773__ $$0PERI:(DE-600)2006039-7$$a10.1021/jp502347b$$gVol. 118, no. 27, p. 7618 - 7629$$n27$$p7618 - 7629$$tThe @journal of physical chemistry <Washington, DC> / B$$v118$$x1520-6106$$y2014
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