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@ARTICLE{Vitova:168874,
author = {Vitova, Tonya and Mangold, S. and Paulmann, Carsten and
Gospodinov and Marinova and Mihailova, Boriana},
title = {{X}-ray absorption spectroscopy of {R}u-doped relaxor
ferroelectrics with a perovskite-type structure},
journal = {Physical review / B},
volume = {89},
number = {14},
issn = {1098-0121},
address = {College Park, Md.},
publisher = {APS},
reportid = {DESY-2014-02701},
pages = {144112},
year = {2014},
abstract = {X-ray absorption near-edge structure and extended x-ray
absorption fine structure spectroscopy at the Ru K edge of
Ru-doped PbSc0.5Ta0.5O3 (PST-Ru), PbSc0.5Nb0.5O3 (PSN-Ru),
and 0.9PbZn1/3Nb2/3O3-0.1PbTiO3 (PZN-0.1PT-Ru) as well as at
the Ta L3 edge of PST-Ru and the Nb K edge of PSN-Ru was
applied to study the short- and intermediate-range atomic
arrangements in perovskite-type (ABO3) relaxor
ferroelectrics. The compounds were also analyzed by
complementary Raman scattering, visible/near-visible
absorption spectroscopy, and synchrotron x-ray
single-crystal diffraction. The results show that Ru is
octahedrally coordinated in all three relaxor host matrices
but the average oxidation state of Ru in PST-Ru and PSN-Ru
is ∼4.4, whereas it is ∼3.8 in PZN-0.1PT-Ru. In
PbSc0.5B''0.5O3 (B'' = Ta, Nb) Ru substitutes for the
B'' cations in the form of isolated point defects, while in
PZN-0.1PT-Ru Ru replaces adjacent A and B sites, forming a
chainlike structural species of face-sharing elongated
octahedra. Chemical 1:1 B-site order as well as dynamic BO6
tilting is observed around both the Ru dopant and the major
B'' cation in PST-Ru and PSN-Ru regardless of the fact that
according to x-ray diffraction at ambient conditions, the
average structure is cubic with weak or no long-range
chemical order. Pb cations are off-center displaced from the
prototypic cubic A site for all three compounds and in
Ru-doped PbSc0.5B''0.5O3 the BO6 tilt angle correlates with
the degree of coherent B-Pb distances.},
cin = {DOOR},
ddc = {530},
cid = {I:(DE-H253)HAS-User-20120731},
pnm = {DORIS Beamline F1 (POF2-54G13) / FS-Proposal: II-20100039
(II-20100039)},
pid = {G:(DE-H253)POF2-F1-20130405 / G:(DE-H253)II-20100039},
experiment = {EXP:(DE-H253)D-F1-20150101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000335228100002},
doi = {10.1103/PhysRevB.89.144112},
url = {https://bib-pubdb1.desy.de/record/168874},
}