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@ARTICLE{Serghiou:166786,
      author       = {Serghiou, G. and Odling, N. and Hunter, R. and Abbie, A.
                      and Armstrong, B. and Lathe, C.},
      title        = {{M}elting and homogeneity in germanium–silicon alloys and
                      a modified micro-manufactured assembly for stable high
                      pressure and temperature measurements},
      journal      = {High pressure research},
      volume       = {34},
      number       = {2},
      issn         = {1477-2299},
      address      = {London [u.a.]},
      publisher    = {Taylor and Francis},
      reportid     = {DESY-2014-01620},
      pages        = {176-183},
      year         = {2014},
      abstract     = {We present a modified assembly for high pressure and
                      temperature measurements in a MAX80 press. Thedesigns
                      include a T-shaped power coupler with a ring-shaped
                      insulator, a precision made, all-in-one singlepiececrucible,
                      with mirror-image located, flat-bottomed sample and pressure
                      marker chambers, with pressfitlids and thermocouple insert
                      in the middle of the crucible. These features facilitate
                      assembly stability,reproducibility of in situ measurements,
                      avoidance of chemical contamination, portability of
                      assemblyand ease of sectioning for further analysis. These
                      attributes are important in evaluating phase relations
                      athigh pressure, especially where melting of the charge is
                      investigated. While the cubic-diamond
                      structuredsilicon–germanium system exhibits a complete
                      solid solution, in practice, homogeneous solid solutionsare
                      not readily accessible because of the considerable
                      difference in temperature between the liquidusand solidus
                      and concomitant segregation coefficients. We use our
                      designs, for in situ X-ray diffractionmeasurements and
                      melting of germanium–silicon alloys at high pressure for
                      both a germanium-rich and asilicon-rich starting
                      composition.},
      cin          = {DOOR / GFZ},
      ddc          = {530},
      cid          = {I:(DE-H253)HAS-User-20120731 / I:(DE-H253)GFZ-20120731},
      pnm          = {DORIS Beamline F2.1 (POF2-54G13)},
      pid          = {G:(DE-H253)POF2-F2.1-20130405},
      experiment   = {EXP:(DE-H253)D-F2.1-20150101},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000337605400003},
      doi          = {10.1080/08957959.2013.856896},
      url          = {https://bib-pubdb1.desy.de/record/166786},
}