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@ARTICLE{Mascotto:92585,
      author       = {Mascotto, S. and Wallacher, D. and Kuschel, A. and Polarz,
                      S. and Zickler, G. A. and Timmann, A. and Smarsly, B. M. and
                      DESY},
      title        = {{A}dsorption in periodically ordered mesoporous
                      organosilica materials studied by in-situ small-angle
                      {X}-ray scattering and small-angle neutron scattering},
      journal      = {Langmuir},
      volume       = {26},
      issn         = {0743-7463},
      address      = {Washington, DC},
      publisher    = {ACS Publ.},
      reportid     = {PHPPUBDB-13027},
      pages        = {6583-6592},
      year         = {2010},
      abstract     = {Modified periodically ordered mesoporous organosilica
                      materials were prepared starting from a recently introduced
                      type of sol-gel precursor, containing both organic moieties
                      and hydrolyzable Si-OR groups. In order to thoroughly
                      characterize the mesoporosity and its accessibility,
                      different probe gases were used in conventional gas
                      adsorption experiments. Furthermore, in situ small-angle
                      X-ray scattering (SAXS) and small-angle neutron scattering
                      (SANS) were applied to study the mesoporosity and the
                      sorption processes, taking advantage of scattering contrast
                      matching conditions. Thereby, the materials were
                      characterized not only by different probe molecules but also
                      at different temperatures (nitrogen at 77 K, dibromomethane
                      at 290 K and perfluoropentane at 276 K). The comparison
                      between the standard and in situ SAXS/SANS adsorption
                      experiments revealed valuable information about the porosity
                      and microstructure of the materials. It is demonstrated that
                      the organic moieties are homogeneously distributed; that is,
                      they do not phase-separate from silica on the nanometer
                      scale.},
      cin          = {HASYLAB},
      ddc          = {670},
      cid          = {$I:(DE-H253)HASYLAB_-2012_-20130307$},
      pnm          = {DORIS Beamline BW4 (POF2-54G13) / FS-Proposal: II-20070030
                      EC (II-20070030-EC)},
      pid          = {G:(DE-H253)POF2-BW4-20130405 / G:(DE-H253)II-20070030-EC},
      experiment   = {EXP:(DE-H253)D-BW4-20150101},
      typ          = {PUB:(DE-HGF)16},
      pubmed       = {pmid:20201568},
      UT           = {WOS:000276969700076},
      doi          = {10.1021/la903934r},
      url          = {https://bib-pubdb1.desy.de/record/92585},
}