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@ARTICLE{Lonsdale:646291,
author = {Lonsdale, Cameron and McMahon, Malcolm},
collaboration = {McHardy, James and Storm, Christian and Glazyrin,
Konstantin and Mezouar, Mohamed},
title = {{A} closer look under extreme pressure: sub-micron
diffraction mapping in a diamond anvil cell},
journal = {High pressure research},
volume = {46},
issn = {0895-7959},
address = {London [u.a.]},
publisher = {Taylor and Francis},
reportid = {PUBDB-2026-00808},
pages = {1 - 26},
year = {2026},
abstract = {Investigating materials under extreme pressure using
diamond anvil cells (DACs) requires very small samples.
X-ray diffraction studies of such samples therefore require
beams focused to <5 μm. Fortuitously, advances in
light-source and beamline design mean that modern
synchrotrons, such as PETRA III and ESRF-EBS, now deliver
sub-μm focusing. Combined with increased source brightness,
fast motors, user-friendly control interfaces, and data
processing advances, 2D mapping of microscopic samples
becomes routine, with exposures on mid-Z samples reduced to
seconds. We demonstrate the use of sub-μm beams, with
high-resolution 2D scans, to map pressure and strain
gradients. We show how small scans are applied to collect
optimum data, and how the sample can affect the pressure
inferred from the pressure calibrant. Although sub-μm beams
can improve compressibility data, they may also introduce
undersampling, revealing variability on μm length scales.
We provide recommendations for the use of sub-μm beams for
extreme conditions research.},
cin = {DOOR ; HAS-User / FS-PET-D},
ddc = {530},
cid = {I:(DE-H253)HAS-User-20120731 /
I:(DE-H253)FS-PET-D-20190712},
pnm = {631 - Matter – Dynamics, Mechanisms and Control
(POF4-631) / 6G3 - PETRA III (DESY) (POF4-6G3) /
FS-Proposal: I-20181032 EC (I-20181032-EC) / FS-Proposal:
I-20211547 (I-20211547) / FS-Proposal: I-20220638
(I-20220638) / FS-Proposal: I-20230886 (I-20230886) /
FS-Proposal: I-20240226 (I-20240226)},
pid = {G:(DE-HGF)POF4-631 / G:(DE-HGF)POF4-6G3 /
G:(DE-H253)I-20181032-EC / G:(DE-H253)I-20211547 /
G:(DE-H253)I-20220638 / G:(DE-H253)I-20230886 /
G:(DE-H253)I-20240226},
experiment = {EXP:(DE-H253)P-P02.2-20150101},
typ = {PUB:(DE-HGF)16},
doi = {10.1080/08957959.2026.2615094},
url = {https://bib-pubdb1.desy.de/record/646291},
}