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@ARTICLE{Karadeniz:429646,
      author       = {Karadeniz, Bahar and Žilić, Dijana and Huskić, Igor and
                      Germann, Luzia S. and Fidelli, Athena M. and Muratović,
                      Senada and Lončarić, Ivor and Etter, Martin and Dinnebier,
                      Robert E. and Barišić, Dajana and Cindro, Nikola and
                      Islamoglu, Timur and Farha, Omar K. and Friscic, Tomislav
                      and Užarević, Krunoslav},
      title        = {{C}ontrolling the {P}olymorphism and {T}opology
                      {T}ransformation in {P}orphyrinic {Z}irconium
                      {M}etal–{O}rganic {F}rameworks via {M}echanochemistry},
      journal      = {Journal of the American Chemical Society},
      volume       = {141},
      number       = {49},
      issn         = {1520-5126},
      address      = {Washington, DC},
      publisher    = {American Chemical Society},
      reportid     = {PUBDB-2019-05166},
      pages        = {19214 - 19220},
      year         = {2019},
      note         = {© American Chemical Society},
      abstract     = {Tetratopic porphyrin-based metal−organicframeworks (MOFs)
                      represent a particularly interestingsubclass of zirconium
                      MOFs due to the occurrence ofseveral divergent topologies.
                      Control over the targettopology is a demanding task, and
                      reports often showproducts containing phase contamination.
                      We demonstratehow mechanochemistry can be exploited
                      forcontrolling the polymorphism in 12-coordinated
                      porphyriniczirconium MOFs, obtaining pure hexagonal
                      PCN-223and cubic MOF-525 phases in 20−60 min of milling.
                      Thereactions are mainly governed by the milling additives
                      andthe zirconium precursor. In situ monitoring by
                      synchrotronpowder X-ray diffraction revealed that
                      specificreaction conditions resulted in the formation of
                      MOF-525 as an intermediate, which rapidly converted to
                      PCN-223 upon milling. Electron spin resonance
                      measurementsrevealed significant differences between the
                      spectra ofparamagnetic centers in two polymorphs, showing
                      apotential of polymorphic Zr-MOFs as tunable supports
                      inspintronics applications.},
      cin          = {DOOR ; HAS-User / FS-PET-D},
      ddc          = {540},
      cid          = {I:(DE-H253)HAS-User-20120731 /
                      I:(DE-H253)FS-PET-D-20190712},
      pnm          = {6G3 - PETRA III (POF3-622) / 6213 - Materials and Processes
                      for Energy and Transport Technologies (POF3-621) /
                      FS-Proposal: I-20150196 (I-20150196)},
      pid          = {G:(DE-HGF)POF3-6G3 / G:(DE-HGF)POF3-6213 /
                      G:(DE-H253)I-20150196},
      experiment   = {EXP:(DE-H253)P-P02.1-20150101},
      typ          = {PUB:(DE-HGF)16},
      pubmed       = {pmid:31747754},
      UT           = {WOS:000502687800005},
      doi          = {10.1021/jacs.9b10251},
      url          = {https://bib-pubdb1.desy.de/record/429646},
}